3-(Cyclohex-1-en-1-yl)thiophene

Base Information

Chemical Name:3-(Cyclohex-1-en-1-yl)thiophene
CAS No.:76441-42-4
Molecular Formula:C10H12S
Molecular Weight:164.271
Hs Code.:
DSSTox Substance ID:DTXSID70505597
Wikidata:Q82360826

Synonyms:76441-42-4;3-(Cyclohex-1-en-1-yl)thiophene;Thiophene-3-yl cyclohexene;SCHEMBL1257292;DTXSID70505597;TXXFGIXDZFZXKD-UHFFFAOYSA-N

Suppliers and Price of 3-(Cyclohex-1-en-1-yl)thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(Cyclohex-1-en-1-yl)thiophene

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:164.06597156
Heavy Atom Count:11
Complexity:160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=CC1)C2=CSC=C2

Technology Process of 3-(Cyclohex-1-en-1-yl)thiophene

There total 4 articles about 3-(Cyclohex-1-en-1-yl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 872-31-1
3-Bromothiophene

: 110-83-8
cyclohexene

: 76441-42-4
1-(3-thiophene-yl)cyclohexene

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; C₁₃H₁₁F₉O₄Pd; N-ethyl-N,N-diisopropylamine; tri tert-butylphosphoniumtetrafluoroborate; at 120 ℃; for 29h; Inert atmosphere; Glovebox; Schlenk technique;
DOI:10.1039/c3cc41722k

Reference yield:

: 6165-69-1
Thien-3-ylboronic acid

: 28075-50-5
cyclohex-1-en-1-yl trifluoromethane sulfonate

: 76441-42-4
1-(3-thiophene-yl)cyclohexene

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; water; at 20 ℃; for 4h;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 76441-42-4
1-(3-thiophene-yl)cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 2 h / -70 °C

2: oxalic acid / toluene

With oxalic acid; In diethyl ether; toluene;
DOI:10.1002/ardp.19803131011