2-{(E)-[(4-Methoxyphenyl)methylidene]amino}-4-nitrophenol

Base Information

Chemical Name:2-{(E)-[(4-Methoxyphenyl)methylidene]amino}-4-nitrophenol
CAS No.:29644-86-8
Molecular Formula:C14H12 N2 O4
Molecular Weight:272.2561
Hs Code.:
NSC Number:112425
DSSTox Substance ID:DTXSID30296878
Mol file:29644-86-8.mol

Synonyms:29644-86-8;NSC112425;DTXSID30296878;2-{(E)-[(4-Methoxyphenyl)methylidene]amino}-4-nitrophenol;AKOS024275138;NSC-112425;2-((4-METHOXY-BENZYLIDENE)-AMINO)-4-NITRO-PHENOL

Suppliers and Price of 2-{(E)-[(4-Methoxyphenyl)methylidene]amino}-4-nitrophenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-{(E)-[(4-Methoxyphenyl)methylidene]amino}-4-nitrophenol

Chemical Property:

Vapor Pressure:1.09E-10mmHg at 25°C
Boiling Point:501.7°Cat760mmHg
Flash Point:257.2°C
Density:1.27g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:272.07970687
Heavy Atom Count:20
Complexity:348

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=NC2=C(C=CC(=C2)[N+](=O)[O-])O

Technology Process of 2-{(E)-[(4-Methoxyphenyl)methylidene]amino}-4-nitrophenol

There total 3 articles about 2-{(E)-[(4-Methoxyphenyl)methylidene]amino}-4-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 99-57-0
2-hydroxy-5-nitroaniline

: 29644-86-8
2-(4-methoxy-benzylidenamino)-4-nitro-phenol

Guidance literature:: In methanol; Heating;
DOI:10.1007/BF00758840

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 29644-86-8
2-(4-methoxy-benzylidenamino)-4-nitro-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / 48 h / Reflux

2: acetic acid / ethanol / 12 h / Reflux; Inert atmosphere

With potassium carbonate; acetic acid; potassium iodide; In ethanol; acetone;
DOI:10.1016/j.tet.2011.08.048