(+/-)-ALPHA-DAMASCONE

Base Information

Chemical Name:(+/-)-ALPHA-DAMASCONE
CAS No.:57549-92-5
Molecular Formula:C₁₃H₂₀O
Molecular Weight:192.301
Hs Code.:
Mol file:57549-92-5.mol

Synonyms:2-Buten-1-one,1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-,(Z);(2)-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one;1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-but-2-en-1-one;(Z)-1-(2,6,6-Trimethyl-2-cyclohexen-1-yl)-2-buten-1-one;1-(2,6,6-Trimethyl-2-cyclohexen-1-yl)-2-buten-1-one;4-(2,6,6-trimethyl-2-cyclohexenyl)-2-butene-4-one;

Suppliers and Price of (+/-)-ALPHA-DAMASCONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-(2.6.6-TRIMETHYL CYCLOHEX-2-ENYL)-BUT-2-EN-4-ONE 95.00%
10G
$ 1334.03

Total 3 raw suppliers

Chemical Property of (+/-)-ALPHA-DAMASCONE

Chemical Property:

Boiling Point:267.1°Cat760mmHg
Flash Point:105.7°C
PSA：17.07000
Density:0.898g/cm³
LogP:3.51410

Purity/Quality:

99.3% ^*data from raw suppliers

4-(2.6.6-TRIMETHYL CYCLOHEX-2-ENYL)-BUT-2-EN-4-ONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (+/-)-ALPHA-DAMASCONE

There total 20 articles about (+/-)-ALPHA-DAMASCONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.7%

: 39900-15-7
(+/-)-3-hydroxy-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

: 57549-92-5,57549-93-6,43052-87-5
⁽²⁾-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

Guidance literature:: With acetic acid; In toluene; at 60 ℃; for 4h;

Reference yield: 83.0%

: 28102-24-1,28102-25-2,52610-46-5,145774-37-4,148021-15-2,148021-16-3
(Z)-2,6,6-Trimethyl-α-(1-propenyl)-2-cyclohexene-1-methanol

: 127-41-3,6901-97-9,14398-36-8,24190-29-2,30685-95-1,31798-12-6,52340-45-1,67529-94-6,67529-95-7
alpha-ionone

: 57549-92-5,57549-93-6,43052-87-5
⁽²⁾-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

Guidance literature:: With Dess-Martin periodane; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)81022-X

Reference yield: 71.0%

: 61899-98-7
2,6,6-trimethylcyclohex-2-en-1-ylidene ketene

: 107-05-1
3-chloroprop-1-ene

: 57549-92-5,57549-93-6,43052-87-5
⁽²⁾-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

Guidance literature:: 3-chloroprop-1-ene; With magnesium; In tetrahydrofuran; at 20 - 42 ℃; for 1h;

2,6,6-trimethylcyclohex-2-en-1-ylidene ketene; In tetrahydrofuran; at 25 ℃; for 1h;

With toluene-4-sulfonic acid; In ethyl acetate; for 12h; Inert atmosphere; Reflux;