2,3-Dimethoxy-4-methylbenzoic acid

Base Information

Chemical Name:2,3-Dimethoxy-4-methylbenzoic acid
CAS No.:77869-39-7
Molecular Formula:C10H12O4
Molecular Weight:196.203
Hs Code.:
DSSTox Substance ID:DTXSID80504359
Wikidata:Q82358806

Synonyms:2,3-dimethoxy-4-methylbenzoic acid;77869-39-7;SCHEMBL6646160;DTXSID80504359;2,3-dimethoxy-4-methylbenzoicacid;FT-0730080;EN300-1697238

Suppliers and Price of 2,3-Dimethoxy-4-methylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Dimethoxy-4-methylbenzoic acid

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:196.07355886
Heavy Atom Count:14
Complexity:204

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1)C(=O)O)OC)OC

Technology Process of 2,3-Dimethoxy-4-methylbenzoic acid

There total 5 articles about 2,3-Dimethoxy-4-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 124-38-9,18923-20-1
carbon dioxide

: 4463-33-6
1,2-dimethoxy-3-methylbenzene

: 77869-39-7
2,3-dimethoxy-4-methylbenzoic acid

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; for 18h; Ambient temperature;
DOI:10.1021/jo00334a053

Reference yield: 12.0%

: 3929-89-3
2,3-dihydroxy-4-methylbenzoic acid

: 77-78-1
dimethyl sulfate

: 77869-39-7
2,3-dimethoxy-4-methylbenzoic acid

: 77869-40-0
2-hydroxy-3-methoxy-4-methylbenzoic acid

Guidance literature:: With sodium hydroxide; In water; at 45 ℃; for 4h;

Reference yield:

: 3929-89-3
2,3-dihydroxy-4-methylbenzoic acid

: 77-78-1
dimethyl sulfate

: 77869-39-7
2,3-dimethoxy-4-methylbenzoic acid

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1) acetone, 24 h, reflux; 2) reflux, 10 h, water;
DOI:10.1021/ja00216a019