1-Methyl-2-(2-pyridyl)pyridinium Iodide

Base Information

• Chemical Name: 1-Methyl-2-(2-pyridyl)pyridinium Iodide
• CAS No.: 77972-47-5
• Molecular Formula: C11H11N2.I
• Molecular Weight: 298.126
• European Community (EC) Number: 833-746-8
• Mol file: 77972-47-5.mol

Synonyms:1-Methyl-2-(2-pyridyl)pyridinium Iodide;77972-47-5;CDA97247;MFCD23700876;AKOS030260398;1-Methyl-2-(2-pyridyl)pyridiniumIodide;1-Methyl-2-pyridin-2-ylpyridinium iodide;1-methyl-[2,2'-bipyridin]-1-ium iodide;CS-0118034;M2778;T72938;10.14272/PIKLCVQDBVTHFG-UHFFFAOYSA-M.1;doi:10.14272/PIKLCVQDBVTHFG-UHFFFAOYSA-M.1

Chemical Property of 1-Methyl-2-(2-pyridyl)pyridinium Iodide

Chemical Property:

• Melting Point: 147.0 to 151.0 °C
• PSA: 16.77000
• LogP: -0.42470
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 297.99670
• Heavy Atom Count: 14
• Complexity: 158

Purity/Quality:

97% ^*data from raw suppliers

1-Methyl-2-(2-pyridyl)pyridinium Iodide >98.0%(HPLC)(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=CC=CC=C1C2=CC=CC=N2.[I-]

Technology Process of 1-Methyl-2-(2-pyridyl)pyridinium Iodide

There total 2 articles about 1-Methyl-2-(2-pyridyl)pyridinium Iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

[2,2]bipyridinyl (366-18-7) + methyl iodide (74-88-4) → 1-methyl-2-(2′-pyridyl)pyridinium iodide (77972-47-5)

Guidance literature:

In acetonitrile; at 45 ℃; for 72h;

DOI:10.3762/bjoc.8.116

Reference yield: 47.0%

[2,2]bipyridinyl (366-18-7) + methyl iodide (74-88-4) → 1-methyl-2-(2′-pyridyl)pyridinium iodide (77972-47-5) + 1,1'-dimethyl-[2,2'-bipyridine]-1,1'-diium iodide (23484-62-0)

Guidance literature:

In acetonitrile; at 45 ℃; for 72h;

DOI:10.3891/acta.chem.scand.52-0077

Reference yield: 88.0%

1-methyl-2-(2′-pyridyl)pyridinium iodide (77972-47-5) → 1-methyl-2,2'-bipyridine-6-one (154928-15-1)

Guidance literature:

With sodium hydroxide; potassium hexacyanoferrate(III); 1.) 10 deg C, 2 h, 2.) RT, 15 h;

upstream raw materials:

[2,2]bipyridinyl

methyl iodide

Downstream raw materials:

[2,2]bipyridinyl

1-methyl-2,2'-bipyridine-6-one

2-bromo-6-(pyridin-2-yl)pyridine

6-Chloro-[2,2']bipyridinyl

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