1-[(4-Methoxyphenyl)methyl]pyridin-1-ium perchlorate

Base Information

• Chemical Name: 1-[(4-Methoxyphenyl)methyl]pyridin-1-ium perchlorate
• CAS No.: 77984-74-8
• Molecular Formula: C13H14NO.ClO4
• Molecular Weight: 299.711
• DSSTox Substance ID: DTXSID20520952
• Mol file: 77984-74-8.mol

Synonyms:77984-74-8;1-[(4-Methoxyphenyl)methyl]pyridin-1-ium perchlorate;DTXSID20520952

Chemical Property of 1-[(4-Methoxyphenyl)methyl]pyridin-1-ium perchlorate

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 299.0560502
• Heavy Atom Count: 20
• Complexity: 265

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C[N+]2=CC=CC=C2.[O-]Cl(=O)(=O)=O

Technology Process of 1-[(4-Methoxyphenyl)methyl]pyridin-1-ium perchlorate

There total 5 articles about 1-[(4-Methoxyphenyl)methyl]pyridin-1-ium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

pyridine (110-86-1) + 1-(p-Methoxybenzyl)-2,4,6-triphenylpyridinium Perchlorate → 1-(p-Methoxybenzyl)pyridinium Perchlorate (77984-74-8)

Guidance literature:

at 100 ℃; for 1h;

Reference yield: 84.0%

1-(p-Methoxybenzyl)-2,4,6-triphenylpyridinium Perchlorate → 1-(p-Methoxybenzyl)pyridinium Perchlorate (77984-74-8)

Guidance literature:

With pyridine; at 100 ℃; for 0.5h;

DOI:10.1021/jo00332a014

Reference yield: 52.0%

pyridine (110-86-1) + 4-Methoxybenzyl alcohol (105-13-5) → 1-(p-Methoxybenzyl)pyridinium Perchlorate (77984-74-8)

Guidance literature:

With perchloric acid; p-toluenesulfonyl chloride; for 1h; Heating;

upstream raw materials:

pyridine

4-Methoxybenzyl alcohol

4-methoxy-benzylamine

p-methylanizole