1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-[(2,4,6-trimethylphenyl)[2,4,6-tris[bis(trimethylsilyl) methyl]phenyl]silyl]-

Base Information

Chemical Name:1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-[(2,4,6-trimethylphenyl)[2,4,6-tris[bis(trimethylsilyl) methyl]phenyl]silyl]-
CAS No.:781640-94-6
Molecular Formula:C₄₂H₈₃BO₂Si₇
Molecular Weight:827.529
Hs Code.:

Synonyms:

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Chemical Property of 1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-[(2,4,6-trimethylphenyl)[2,4,6-tris[bis(trimethylsilyl) methyl]phenyl]silyl]-

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Technology Process of 1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-[(2,4,6-trimethylphenyl)[2,4,6-tris[bis(trimethylsilyl) methyl]phenyl]silyl]-

There total 4 articles about 1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-[(2,4,6-trimethylphenyl)[2,4,6-tris[bis(trimethylsilyl) methyl]phenyl]silyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 185910-18-3
1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 781640-94-6
2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)silylpinacolborane

Guidance literature:: In tetrahydrofuran; (Ar); heating a mixt. of silicon and boron compds. in THF at 60°Cin a sealed tube for 16.5 h; evapn., dissolving in hexane, filtration through Celite, evapn. HPLC (LC-918, CHCl3);
DOI:10.1021/om049558w

Reference yield: 25.0%

: 3282-30-2
pivaloyl chloride

: 796870-05-8
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2

: 781640-94-6
2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)silylpinacolborane

: 781640-95-7
2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)chlorosilylpinacolborane

Guidance literature:: With n-BuLi; In hexane; (Ar); soln. of BuLi in hexane was added to soln. of B compd. in hexane at 0°C; stirred at 0°C for 30 min; chloride was added at 0°C; stirred at 0°C for 30 min and overnight, while warmed to room temp.; solvent removed; chromd. (SiO2 plate, hexane/CHCl3, 3/2);
DOI:10.1021/om7008974

Reference yield: 9.0%

: 185910-20-7
2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiCN(2,4,6-triisopropylphenyl)

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 781640-94-6
2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)silylpinacolborane

: ((CH₃)2CH)3C₆H₂NCBO₂C₂(CH₃)4SiH(C₆H₂(CH₃)3)(C₆H₂(CH(Si(CH₃)3)2)3)

Guidance literature:: In benzene-d6; (Ar); addn. of boron compd. to a soln. of silicon compd. in C6D6 at 0°C, sealing, standing for 2 wk at room temp.; evapn., HPLC (LC-918, CHCl3);
DOI:10.1021/om049558w