(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2

Base Information

• Chemical Name: (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2
• CAS No.: 796870-05-8
• Molecular Formula: C₄₈H₉₄B₂O₄Si₇
• Molecular Weight: 953.492

Synonyms:(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2

Chemical Property of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2

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Technology Process of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2

There total 3 articles about (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

bis(pinacol)diborane (73183-34-3) + (Z)-1,2-dimesityl-1,2-bis{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}disilene → (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2 (796870-05-8)

Guidance literature:

In tetrahydrofuran; at 60 ℃; for 120h;

DOI:10.1039/b409575h

Reference yield: 45.0%

1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene (185910-18-3) + bis(pinacol)diborane (73183-34-3) → (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2 (796870-05-8)

Guidance literature:

In not given; heated at 60°C for 5 d in THF or benzene; chromy. (silica gel);

DOI:10.1039/b409575h

Reference yield: 12.0%

bis(pinacol)diborane (73183-34-3) + 2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiCN(2,4,6-tri-tert-butylphenyl) → (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2 (796870-05-8)

Guidance literature:

In not given; heated at 80°C for 3 d;

DOI:10.1039/b409575h

upstream raw materials:

bis(pinacol)diborane

1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene

Downstream raw materials:

(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

(C₆H₂(CH₃)3)(C₆H₂(CH(Si(CH₃)3)2)2C(Si(CH₃)3)2)SiH(BOC(CH₃)2C(CH₃)2OH)

2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)silylpinacolborane

2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)chlorosilylpinacolborane

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