Benzenamine, 4-bromo-2-nitro-6-(2-pyrimidinyl)-

Base Information

Chemical Name:Benzenamine, 4-bromo-2-nitro-6-(2-pyrimidinyl)-
CAS No.:797047-19-9
Molecular Formula:C10H7BrN4O2
Molecular Weight:295.095
Hs Code.:

Synonyms:4-bromo-2-nitro-6-pyrimidin-2-yl-phenylamine;4-bromo-2-nitro-6-(pyrimidin-2-yl)phenylamine;4-bromo-2-nitro-6-pyrimidin-2-yl-phenylanine;

Suppliers and Price of Benzenamine, 4-bromo-2-nitro-6-(2-pyrimidinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzenamine, 4-bromo-2-nitro-6-(2-pyrimidinyl)-

Chemical Property:

PSA：97.62000
LogP:3.50090

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenamine, 4-bromo-2-nitro-6-(2-pyrimidinyl)-

There total 3 articles about Benzenamine, 4-bromo-2-nitro-6-(2-pyrimidinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 797047-18-8
N-(4-bromo-2-nitro-6-pyrimidin-2-yl-phenyl)-2,2-dimethyl-propionamide

: 797047-19-9
4-bromo-2-nitro-6-(pyrimidin-2-yl)benzenamine

Guidance literature:: With hydrogenchloride; In ethanol; at 80 - 88 ℃; for 58.5h; Heating / reflux;

Reference yield:

: 1073354-10-5
2,2-dimethyl-N-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propionamide

: 797047-19-9
4-bromo-2-nitro-6-(pyrimidin-2-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 100 °C

2.1: bromine; sodium acetate / acetic acid

2.3: Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; sodium acetate; sodium carbonate; In 1,2-dimethoxyethane; water; acetic acid;
DOI:10.1016/j.bmcl.2014.03.022

Reference yield:

: 797047-16-6
2,2-dimethyl-N-(2-pyrimidin-2-yl-phenyl)-propionamide

: 797047-19-9
4-bromo-2-nitro-6-(pyrimidin-2-yl)benzenamine

Guidance literature:: 2,2-dimethyl-N-(2-pyrimidin-2-yl-phenyl)-propionamide; With bromine; sodium acetate; In acetic acid;

With sulfuric acid; nitric acid; trifluoroacetic acid;

With hydrogenchloride; In water; Reflux;
DOI:10.1016/j.bmcl.2014.03.022