N,N'-BIS(METHOXYMETHYL)DIAZA-18-CROWN-6

Base Information

• Chemical Name: N,N'-BIS(METHOXYMETHYL)DIAZA-18-CROWN-6
• CAS No.: 83809-94-3
• Molecular Formula: C16H34 N2 O6
• Molecular Weight: 350.456
• Hs Code.: 29349990
• Mol file: 83809-94-3.mol

Synonyms:N,N’-BIS(METHOXYMETHYL)DIAZA-18-CROWN-6;N,N’-BIS(METHOXYMETHYL)DIAZA-18-CROWN-6 97%

Chemical Property of N,N'-BIS(METHOXYMETHYL)DIAZA-18-CROWN-6

Chemical Property:

• Vapor Pressure: 4.31E-08mmHg at 25°C
• Melting Point: 33-38 °C
• Refractive Index: 1.5500 (estimate)
• Boiling Point: 444.4°C at 760 mmHg
• Flash Point: 122.7°C
• PSA: 64.26000
• Density: 1.0637 (rough estimate)
• LogP: 0.18240

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-BIS(METHOXYMETHYL)DIAZA-18-CROWN-6

There total 2 articles about N,N'-BIS(METHOXYMETHYL)DIAZA-18-CROWN-6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1,4,10,13-tetraoxa-7,16-diazacyclooctadecane (23978-55-4) → 1,10-bis(methoxymethyl)-1,10-diaza-18-crown-6 (83809-94-3)

Guidance literature:

In methanol; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/ejic.201201564

Reference yield:

methanol (67-56-1) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1,4,10,13-tetraoxa-7,16-diazacyclooctadecane (23978-55-4) → 1,10-bis(methoxymethyl)-1,10-diaza-18-crown-6 (83809-94-3)

Guidance literature:

at 20 ℃; for 12h;

Reference yield: 100.0%

N,N-dimethoxyamine (88470-26-2) + 1,10-bis(methoxymethyl)-1,10-diaza-18-crown-6 (83809-94-3) → C18H40N4O8

Guidance literature:

In diethyl ether; for 5h; Heating;

DOI:10.1007/BF00955378

upstream raw materials:

methanol

formaldehyd

1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

Downstream raw materials:

N,N'-Bis(N-benzyl-p-toluenesulfonamidomethyl)diaza-18-crown-6

N,N'-Bis(N-tosylethoxycarbonylmethylaminomethyl)diaza-18-crown-6

7,16-Bis(2-hydroxyphenylmethyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

N,N'-Bis(N-methyl-p-toluenesulfonamidomethyl)diaza-18-crown-6