Diphenyl{2-[(trimethylsilyl)oxy]phenyl}phosphane

Base Information

Chemical Name:Diphenyl{2-[(trimethylsilyl)oxy]phenyl}phosphane
CAS No.:81323-70-8
Molecular Formula:C21H23OPSi
Molecular Weight:350.472
Hs Code.:
DSSTox Substance ID:DTXSID70573635
Nikkaji Number:J1.078.328C

Synonyms:81323-70-8;Diphenyl{2-[(trimethylsilyl)oxy]phenyl}phosphane;DTXSID70573635

Suppliers and Price of Diphenyl{2-[(trimethylsilyl)oxy]phenyl}phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Diphenyl{2-[(trimethylsilyl)oxy]phenyl}phosphane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:350.12557889
Heavy Atom Count:24
Complexity:351

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)OC1=CC=CC=C1P(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Diphenyl{2-[(trimethylsilyl)oxy]phenyl}phosphane

There total 3 articles about Diphenyl{2-[(trimethylsilyl)oxy]phenyl}phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 60254-10-6
(o-hydroxyphenyl)diphenylphosphine

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 81323-70-8
diphenyl(2-trimethylsiloxyphenyl)phosphine

Guidance literature:: With chloro-trimethyl-silane; In methyl cyclohexane; at 100 ℃; for 16h;

Reference yield:

: 53111-20-9
(2-methoxyphenyl)diphenylphosphine

: 81323-70-8
diphenyl(2-trimethylsiloxyphenyl)phosphine

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / 48percent HBr / 96 h / Heating

2: 94 percent / Na / ethanol / 5 h / Ambient temperature

3: 99 percent / Me₃ClSi / methylcyclohexane / 16 h / 100 °C

With chloro-trimethyl-silane; hydrogen bromide; sodium; In ethanol; methyl cyclohexane;

Reference yield:

: (2-Hydroxyphenyl)diphenylphosphane hydrobromid

: 81323-70-8
diphenyl(2-trimethylsiloxyphenyl)phosphine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Na / ethanol / 5 h / Ambient temperature

2: 99 percent / Me₃ClSi / methylcyclohexane / 16 h / 100 °C

With chloro-trimethyl-silane; sodium; In ethanol; methyl cyclohexane;