Sulfuric acid, 2,6-difluorophenyl phenyl ester

Base Information

Chemical Name:Sulfuric acid, 2,6-difluorophenyl phenyl ester
CAS No.:820220-75-5
Molecular Formula:C12H8F2O4S
Molecular Weight:286.256
Hs Code.:
DSSTox Substance ID:DTXSID40460629
Nikkaji Number:J2.138.723A
Wikidata:Q82284751

Synonyms:820220-75-5;Sulfuric acid, 2,6-difluorophenyl phenyl ester;DTXSID40460629

Suppliers and Price of Sulfuric acid, 2,6-difluorophenyl phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Sulfuric acid, 2,6-difluorophenyl phenyl ester

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:286.01113623
Heavy Atom Count:19
Complexity:366

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)OS(=O)(=O)OC2=C(C=CC=C2F)F

Technology Process of Sulfuric acid, 2,6-difluorophenyl phenyl ester

There total 2 articles about Sulfuric acid, 2,6-difluorophenyl phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 28177-48-2
2,6-difluorophenol

: 16475-29-9
phenylchlorosulfate

: 820220-75-5
2,6-difluorophenyl phenyl sulfate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1021/jo0488309

Reference yield:

: 100-67-4
potassium phenolate

: 820220-75-5
2,6-difluorophenyl phenyl sulfate

Guidance literature:: Multi-step reaction with 2 steps

1: 17 percent / SO₂Cl₂ / benzene / 0 - 20 °C

2: 9 percent / DBU / tetrahydrofuran / 24 h / 20 °C

With sulfuryl dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; benzene;
DOI:10.1021/jo0488309