Benzamide, N-(4-chloro-2-iodophenyl)-2-nitro-

Base Information

Chemical Name:Benzamide, N-(4-chloro-2-iodophenyl)-2-nitro-
CAS No.:826991-59-7
Molecular Formula:C13H8ClIN2O3
Molecular Weight:402.576
Hs Code.:
DSSTox Substance ID:DTXSID30479543
Wikidata:Q82313638

Synonyms:Benzamide, N-(4-chloro-2-iodophenyl)-2-nitro-;826991-59-7;DTXSID30479543

Suppliers and Price of Benzamide, N-(4-chloro-2-iodophenyl)-2-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzamide, N-(4-chloro-2-iodophenyl)-2-nitro-

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:401.92682
Heavy Atom Count:20
Complexity:377

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NC2=C(C=C(C=C2)Cl)I)[N+](=O)[O-]

Technology Process of Benzamide, N-(4-chloro-2-iodophenyl)-2-nitro-

There total 2 articles about Benzamide, N-(4-chloro-2-iodophenyl)-2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 63069-48-7
p-chloro-o-iodoaniline

: 610-14-0
2-nitrobenzyl chloride

: 826991-59-7
N-(4-chloro-2-iodo-phenyl)-2-nitro-benzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1016/j.tet.2004.10.061

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 826991-59-7
N-(4-chloro-2-iodo-phenyl)-2-nitro-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 3 h / 0 - 75 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

2.2: 5 h / 20 °C / Inert atmosphere

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/adsc.201600748

Reference yield: 88.0%

: 77-78-1
dimethyl sulfate

: 826991-59-7
N-(4-chloro-2-iodo-phenyl)-2-nitro-benzamide

: 826991-85-9
2-chloro-N-methyl-N-(2-nitro-phenyl)-pyridine-3-carboxamide

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In benzene; at 70 - 80 ℃; for 12h;
DOI:10.1016/j.tet.2004.10.061