Silane, (1,1-dimethylethyl)[(3-ethenyl-2-methyl-1-cyclohexen-1-yl)oxy]dimethyl-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)[(3-ethenyl-2-methyl-1-cyclohexen-1-yl)oxy]dimethyl-
CAS No.:827007-83-0
Molecular Formula:C15H28OSi
Molecular Weight:252.46800
Hs Code.:

Synonyms:tert-Butyl-dimethyl-(2-methyl-3-vinyl-cyclohex-1-enyloxy)-silane;

Suppliers and Price of Silane, (1,1-dimethylethyl)[(3-ethenyl-2-methyl-1-cyclohexen-1-yl)oxy]dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, (1,1-dimethylethyl)[(3-ethenyl-2-methyl-1-cyclohexen-1-yl)oxy]dimethyl-

Chemical Property:

PSA：9.23000
LogP:5.26830

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Silane, (1,1-dimethylethyl)[(3-ethenyl-2-methyl-1-cyclohexen-1-yl)oxy]dimethyl-

There total 1 articles about Silane, (1,1-dimethylethyl)[(3-ethenyl-2-methyl-1-cyclohexen-1-yl)oxy]dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1121-18-2
2-methyl-2-cyclohexen-1-one

: 1826-67-1
vinyl magnesium bromide

: 18162-48-6
tert-butyldimethylsilyl chloride

: 827007-83-0
tert-butyldimethyl-(2-methyl-3-vinyl-cyclohex-1-enyloxy)-silane

Guidance literature:: vinyl magnesium bromide; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -40 ℃; for 0.25h;

2-methyl-2-cyclohexen-1-one; tert-butyldimethylsilyl chloride; In tetrahydrofuran; at -40 - -20 ℃; for 1h;

With triethylamine; In tetrahydrofuran; at -20 - 20 ℃;
DOI:10.1016/j.tet.2005.11.056