2-N,N-DIBENZYL SERINE BENZYL ESTER

Base Information

• Chemical Name: 2-N,N-DIBENZYL SERINE BENZYL ESTER
• CAS No.: 82770-40-9
• Molecular Formula: C24H25NO3
• Molecular Weight: 375.467
• Mol file: 82770-40-9.mol

Synonyms:(2S)-N,N-dibenzyl serine benzyl ester;N,N-dibenzyl-L-serine benzyl ester;N,N-DIBENZYL-L-PHENYLALANINE;

Chemical Property of 2-N,N-DIBENZYL SERINE BENZYL ESTER

Chemical Property:

• Vapor Pressure: 1.58E-12mmHg at 25°C
• Refractive Index: n20/D 1.573(lit.)
• Boiling Point: 290oC(lit.)
• Flash Point: 110oC
• PSA: 49.77000
• Density: 1.06 g/mL at 25oC(lit.)
• LogP: 3.79310
• Solubility.: Chloroform, Dichloromethane, Ethanol, Ethyl Acetate, Methanol

Purity/Quality:

99% ^*data from raw suppliers

2-N,N-Dibenzyl Serine Benzyl Ester ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-N,N-Dibenzyl Serine Benzyl Ester is a compound useful in organic synthesis.

Technology Process of 2-N,N-DIBENZYL SERINE BENZYL ESTER

There total 1 articles about 2-N,N-DIBENZYL SERINE BENZYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

L-serin (56-45-1,83245-15-2) + benzyl bromide (100-39-0) → (S)-benzyl 2-(dibenzylamino)-3-hydroxypropanoate (82770-40-9)

Guidance literature:

With potassium hydroxide; potassium carbonate; In ethanol; water; for 0.333333h; Heating;

DOI:10.1021/ja994215o

Reference yield: 92.0%

(S)-benzyl 2-(dibenzylamino)-3-hydroxypropanoate (82770-40-9) → (R)-2-Bromo-3-dibenzylamino-propionic acid benzyl ester

Guidance literature:

With sulfurous dibromide; N,N-dimethyl-formamide; In cyclohexane; at 20 ℃; for 4h;

DOI:10.1016/S0040-4039(00)00330-0

Reference yield: 90.0%

(S)-benzyl 2-(dibenzylamino)-3-hydroxypropanoate (82770-40-9) → N,N-dibenzyl-α-fluoro-β-alanine benzyl ester (887352-80-9)

Guidance literature:

With diethylamino-sulfur trifluoride; In tetrahydrofuran; for 0.5h; Ambient temperature;

DOI:10.1021/ja00385a070

upstream raw materials:

L-serin

benzyl bromide

Downstream raw materials:

N,N-dibenzyl-α-fluoro-β-alanine benzyl ester

(2S)-benzyl 2-(N,N-dibenzylamino)-3-(triphenylmethoxy)propanoate

(2S)-2-(N,N-dibenzylamino)-3-(triphenylmethoxy)propanal

(-)-(2R)-2-[bis(phenylmethyl)amino]-3-(trityloxy)propan-1-ol

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