1-Bromo-2-ethenylcyclohex-1-ene

Base Information

Chemical Name:1-Bromo-2-ethenylcyclohex-1-ene
CAS No.:83043-84-9
Molecular Formula:C8H11Br
Molecular Weight:187.079
Hs Code.:
DSSTox Substance ID:DTXSID90538004
Nikkaji Number:J1.898.237D

Synonyms:83043-84-9;1-Bromo-2-ethenylcyclohex-1-ene;DTXSID90538004

Suppliers and Price of 1-Bromo-2-ethenylcyclohex-1-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-Bromo-2-ethenylcyclohex-1-ene

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:186.00441
Heavy Atom Count:9
Complexity:145

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC1=C(CCCC1)Br

Technology Process of 1-Bromo-2-ethenylcyclohex-1-ene

There total 9 articles about 1-Bromo-2-ethenylcyclohex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 38127-47-8
2-bromocyclohex-1-ene-1-carbaldehyde

: 2065-66-9
methyl-triphenylphosphonium iodide

: 83043-84-9
1-Bromo-2-ethenylcyclohex-1-ene

Guidance literature:: methyl-triphenylphosphonium iodide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.583333h; Inert atmosphere;

2-bromocyclohex-1-ene-1-carbaldehyde; In tetrahydrofuran; hexane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201108027

Reference yield: 82.0%

: 38127-47-8
2-bromocyclohex-1-ene-1-carbaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 83043-84-9
1-Bromo-2-ethenylcyclohex-1-ene

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.5h;

2-bromocyclohex-1-ene-1-carbaldehyde; In tetrahydrofuran; for 1h;
DOI:10.1021/ja0212009

Reference yield: 71.0%

: 7486-35-3
tri-n-butyl(vinyl)tin

: 213340-08-0
1-bromo-2-trifluoromethanesulfonyloxycyclohexene

: 83043-84-9
1-Bromo-2-ethenylcyclohex-1-ene

Guidance literature:: With triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 25 ℃; for 18h;
DOI:10.1002/1521-3765(20010917)7:18<4035::AID-CHEM4035>3.0.CO;2-P