1,2-BIS(TRIMETHOXYSILYL)DECANE

Base Information

Chemical Name:1,2-BIS(TRIMETHOXYSILYL)DECANE
CAS No.:832079-33-1
Molecular Formula:C₁₆H₃₈O₆Si₂
Molecular Weight:382.645
Hs Code.:2931900090
Mol file:832079-33-1.mol

Synonyms:2,7-Dioxa-3,6-disilaoctane,3,3,6,6-tetramethoxy-4-octyl;1,2-BIS(TRIMETHOXYSILYL)DECANE;

Suppliers and Price of 1,2-BIS(TRIMETHOXYSILYL)DECANE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2-BIS(TRIMETHOXYSILYL)DECANE 95.00%
500G
$ 5740.35

American Custom Chemicals Corporation
1,2-BIS(TRIMETHOXYSILYL)DECANE 95.00%
100G
$ 3372.60

American Custom Chemicals Corporation
1,2-BIS(TRIMETHOXYSILYL)DECANE 95.00%
25G
$ 216.30

Total 10 raw suppliers

Chemical Property of 1,2-BIS(TRIMETHOXYSILYL)DECANE

Chemical Property:

Vapor Pressure:0.000138mmHg at 25°C
Refractive Index:1.4303
Boiling Point:130-132oC 0,4mm
Flash Point:140.9oC
PSA：55.38000
Density:0.984 g/cm3
LogP:3.86340

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,2-BIS(TRIMETHOXYSILYL)DECANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-BIS(TRIMETHOXYSILYL)DECANE

There total 3 articles about 1,2-BIS(TRIMETHOXYSILYL)DECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1445-45-0
Trimethyl orthoacetate

: 620987-03-3
1,2-bis(trichlorosilyl)decane

: 149-73-5
trimethyl orthoformate

: 832079-33-1
1,2-bis(trimethoxysilyl)decane

Guidance literature:: 1,2-bis(trichlorosilyl)decane; trimethyl orthoformate; at 100 ℃; pH=6 - 7; Inert atmosphere; Large scale;

Trimethyl orthoacetate; at 120 ℃; Inert atmosphere; Large scale;
DOI:10.1002/chem.201402757

Reference yield:

: 67-56-1
methanol

: 620987-03-3
1,2-bis(trichlorosilyl)decane

: 832079-34-2
1-trichlorosilyl-2-dichlorosilyldecane

: 149-73-5
trimethyl orthoformate

: 832079-33-1
1,2-bis(trimethoxysilyl)decane

Guidance literature:: 1,2-bis(trichlorosilyl)decane; 1-trichlorosilyl-2-dichlorosilyldecane; trimethyl orthoformate; at 40 - 150 ℃;

methanol; dihydrogen hexachloroplatinate; In tetrahydrofuran; at 80 - 120 ℃; for 2h;

Reference yield:

: 872-05-9,17438-89-0,25189-70-2
1-Decene

: 832079-33-1
1,2-bis(trimethoxysilyl)decane

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorosilane; tri(butyl)tetradecylphosphonium chloride / toluene / 18 h / 220 °C / Autoclave; Inert atmosphere; Large scale

2.1: 100 °C / pH 6 - 7 / Inert atmosphere; Large scale

2.2: 120 °C / Inert atmosphere; Large scale

With tri(butyl)tetradecylphosphonium chloride; trichlorosilane; In toluene;
DOI:10.1002/chem.201402757