3-Methyl-6-(3-phenylacryloyl)-1,3-benzoxazol-2(3H)-one

Base Information

Chemical Name:3-Methyl-6-(3-phenylacryloyl)-1,3-benzoxazol-2(3H)-one
CAS No.:83297-64-7
Molecular Formula:C17H13NO3
Molecular Weight:279.295
Hs Code.:
DSSTox Substance ID:DTXSID50706085

Synonyms:83297-64-7;SCHEMBL9196440;3-Methyl-6-(3-phenylacryloyl)-1,3-benzoxazol-2(3H)-one;DTXSID50706085

Suppliers and Price of 3-Methyl-6-(3-phenylacryloyl)-1,3-benzoxazol-2(3H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Methyl-6-(3-phenylacryloyl)-1,3-benzoxazol-2(3H)-one

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:279.08954328
Heavy Atom Count:21
Complexity:439

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)C(=O)C=CC3=CC=CC=C3)OC1=O

Technology Process of 3-Methyl-6-(3-phenylacryloyl)-1,3-benzoxazol-2(3H)-one

There total 1 articles about 3-Methyl-6-(3-phenylacryloyl)-1,3-benzoxazol-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 54903-61-6
6-acetyl-3-methylbenzoxazolinone

: 100-52-7
benzaldehyde

: 83297-64-7
3-Methyl-6-[(E)-(3-phenyl-acryloyl)]-3H-benzooxazol-2-one

Guidance literature:: With hydrogenchloride; In ethanol; for 30h; Ambient temperature;
DOI:10.1080/00397919608003834

Reference yield: 30.0%

: 83297-64-7
3-Methyl-6-[(E)-(3-phenyl-acryloyl)]-3H-benzooxazol-2-one

: 80428-00-8
2,7-dioxo-3-methyl-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole

Guidance literature:: With PPA; at 120 ℃;
DOI:10.1080/00397919608003834

Reference yield:

: 83297-64-7
3-Methyl-6-[(E)-(3-phenyl-acryloyl)]-3H-benzooxazol-2-one

: 134541-21-2
3-methyl-7-oximino-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / polyphosphoric acid / 120 °C

2: 60 percent / NH₂OH*HCl, K₂CO₃ / ethanol; H₂O / 3 h / Heating

With PPA; hydroxylamine hydrochloride; potassium carbonate; In ethanol; water;
DOI:10.1080/00397919608003834