N,N-Dimethyl-2-[(trimethylstannyl)methyl]aniline

Base Information

• Chemical Name: N,N-Dimethyl-2-[(trimethylstannyl)methyl]aniline
• CAS No.: 84457-45-4
• Molecular Formula: C₁₂H₂₁NSn
• Molecular Weight: 298.015
• DSSTox Substance ID: DTXSID90514843
• Wikidata: Q82375390

Synonyms:84457-45-4;N,N-Dimethyl-2-[(trimethylstannyl)methyl]aniline;DTXSID90514843

Chemical Property of N,N-Dimethyl-2-[(trimethylstannyl)methyl]aniline

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 299.069602
• Heavy Atom Count: 14
• Complexity: 172

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=CC=C1C[Sn](C)(C)C

Technology Process of N,N-Dimethyl-2-[(trimethylstannyl)methyl]aniline

There total 2 articles about N,N-Dimethyl-2-[(trimethylstannyl)methyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

trimethyltin(IV)chloride (1066-45-1) + 2-(dimethylamino)benzyllithium (64308-58-3) → C6H4(N(CH3)2)CH2Sn(CH3)3 (84457-45-4)

Guidance literature:

In diethyl ether; byproducts: LiCl; N2-atmosphere;

Reference yield: 58.0%

trimethyltin bromide (1066-44-0) + 2-(dimethylamino)benzyllithium (64308-58-3) → C6H4(N(CH3)2)CH2Sn(CH3)3 (84457-45-4)

Guidance literature:

In tetrahydrofuran; a soln. of Me3SnBr was added to a soln. of organolithium, stirred for 2h at room temp.; hydrolysis, distillation;

DOI:10.1016/S0022-328X(00)84800-7

Reference yield:

C6H4(N(CH3)2)CH2Sn(CH3)3 (84457-45-4) → C6H4(N(CH3)2)CH2Sn(CH3)2I (112379-36-9)

Guidance literature:

With iodine; In not given; iododemetallation carried out in CDCl3 or C6D6, in the dark;

DOI:10.1039/c39870000513

upstream raw materials:

trimethyltin bromide

2-(dimethylamino)benzyllithium

trimethyltin(IV)chloride

Downstream raw materials:

C₆H₄(N(CH₃)2)CH₂Sn(CH₃)2I

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