1,17-Bis(4-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane

Base Information

Chemical Name:1,17-Bis(4-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane
CAS No.:84649-38-7
Molecular Formula:C24H32N2O11
Molecular Weight:524.525
Hs Code.:
DSSTox Substance ID:DTXSID30517358
Wikidata:Q82379324

Synonyms:84649-38-7;DTXSID30517358;1,17-BIS(4-NITROPHENOXY)-3,6,9,12,15-PENTAOXAHEPTADECANE

Suppliers and Price of 1,17-Bis(4-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,17-Bis(4-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:11
Rotatable Bond Count:20
Exact Mass:524.20060984
Heavy Atom Count:37
Complexity:536

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1[N+](=O)[O-])OCCOCCOCCOCCOCCOCCOC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 1,17-Bis(4-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane

There total 3 articles about 1,17-Bis(4-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.2%

: 824-78-2
4-nitrophenol sodium salt

: 52559-90-7,27252-69-3
1,17-dichloro-3,6,9,12,15-pentaoxaheptadecane

: 84649-38-7
1,17-bis(p-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane

Guidance literature:: In sulfolane; at 150 ℃; for 30h;
DOI:10.1021/ja00345a029

Reference yield: 74.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 42749-27-9
hexa(ethyleneglycol) ditosylate

: 84649-38-7
1,17-bis(p-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane

Guidance literature:: With potassium carbonate; In acetonitrile; for 8h; Inert atmosphere; Reflux;
DOI:10.1039/c6cc03144g

Reference yield:

: 2615-15-8
pentaethylene glycol

: 84649-38-7
1,17-bis(p-nitrophenoxy)-3,6,9,12,15-pentaoxaheptadecane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / tetrahydrofuran; water / 7 h / Cooling with ice

2: potassium carbonate / acetonitrile / 8 h / Inert atmosphere; Reflux

With potassium carbonate; potassium hydroxide; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c6cc03144g