Technology Process of Benzenemethanol, 2-(dimethylsilyl)-, acetate
There total 7 articles about Benzenemethanol, 2-(dimethylsilyl)-, acetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole;
With
lithium aluminium tetrahydride;
In
diethyl ether;
at 20 ℃;
for 1.66667h;
acetyl chloride;
In
diethyl ether;
at 0 - 20 ℃;
DOI:10.1021/ja051281j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 83 percent / p-toluenesulfonic acid monohydrate / methanol / 16 h / 20 °C
2: LiAlH4 / diethyl ether / 1.67 h / 20 °C
3: diethyl ether / 0 - 20 °C
With
lithium aluminium tetrahydride; toluene-4-sulfonic acid;
In
methanol; diethyl ether;
DOI:10.1016/j.jorganchem.2006.04.046
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 0.67 h / -78 °C
1.2: 83 percent / tetrahydrofuran; hexane / -78 - 20 °C
2.1: 83 percent / p-toluenesulfonic acid monohydrate / methanol / 16 h / 20 °C
3.1: LiAlH4 / diethyl ether / 1.67 h / 20 °C
4.1: diethyl ether / 0 - 20 °C
With
lithium aluminium tetrahydride; n-butyllithium; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; diethyl ether; hexane;
DOI:10.1016/j.jorganchem.2006.04.046