4-{[(Trimethylsilyl)oxy]methyl}morpholine

Base Information

• Chemical Name: 4-{[(Trimethylsilyl)oxy]methyl}morpholine
• CAS No.: 85413-82-7
• Molecular Formula: C8H19NO2Si
• Molecular Weight: 189.33
• DSSTox Substance ID: DTXSID70515691
• Wikidata: Q82376708

Synonyms:85413-82-7;4-{[(Trimethylsilyl)oxy]methyl}morpholine;DTXSID70515691

Chemical Property of 4-{[(Trimethylsilyl)oxy]methyl}morpholine

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 189.118505383
• Heavy Atom Count: 12
• Complexity: 130

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)OCN1CCOCC1

Technology Process of 4-{[(Trimethylsilyl)oxy]methyl}morpholine

There total 1 articles about 4-{[(Trimethylsilyl)oxy]methyl}morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

4-(trimethylsilyl)morpholine (13368-42-8) + formaldehyd (50-00-0,30525-89-4,61233-19-0) → 4-(morpholinomethyl)morpholine (5625-90-1) + Hexamethyldisiloxane (107-46-0) + trimethyl(morpholinomethoxy)silane (85413-82-7)

Guidance literature:

at 25 - 30 ℃; for 1h;

Reference yield: 88.0%

N-trimethylsilyl-pyrrolidin-2-one (14468-90-7) + trimethyl(morpholinomethoxy)silane (85413-82-7) → 4-<(2-oxo-1-pyrrolidinyl)methyl>morpholine (34609-03-5) + Hexamethyldisiloxane (107-46-0)

Guidance literature:

trimethylsilyl iodide; In diethyl ether; for 72h; Ambient temperature;

Reference yield: 70.0%

4-(trimethylsilyl)morpholine (13368-42-8) + trimethyl(morpholinomethoxy)silane (85413-82-7) → 4-(morpholinomethyl)morpholine (5625-90-1) + Hexamethyldisiloxane (107-46-0)

Guidance literature:

at 30 ℃; for 1h;

upstream raw materials:

4-(trimethylsilyl)morpholine

formaldehyd

Downstream raw materials:

4-(morpholinomethyl)morpholine

Hexamethyldisiloxane

4-<(2-oxo-1-pyrrolidinyl)methyl>morpholine

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