Ethyl 2-phenylprop-2-en-1-yl carbonate

Base Information

Chemical Name:Ethyl 2-phenylprop-2-en-1-yl carbonate
CAS No.:86537-63-5
Molecular Formula:C12H14O3
Molecular Weight:206.241
Hs Code.:
DSSTox Substance ID:DTXSID20524091
Wikidata:Q82390703

Synonyms:86537-63-5;Ethyl 2-phenylprop-2-en-1-yl carbonate;DTXSID20524091

Suppliers and Price of Ethyl 2-phenylprop-2-en-1-yl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Ethyl 2-phenylprop-2-en-1-yl carbonate

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:206.094294304
Heavy Atom Count:15
Complexity:217

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)OCC(=C)C1=CC=CC=C1

Technology Process of Ethyl 2-phenylprop-2-en-1-yl carbonate

There total 1 articles about Ethyl 2-phenylprop-2-en-1-yl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 6006-81-1
3-hydroxy-2-phenylpropene

: 541-41-3
chloroformic acid ethyl ester

: 86537-63-5
Ethyl 2-Phenyl-2-propenyl carbonate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/acs.orglett.9b01497

Reference yield: 95.0%

: 4648-54-8
trimethylsilylazide

: 86537-63-5
Ethyl 2-Phenyl-2-propenyl carbonate

: 128318-85-4
1-(1-azidoprop-2-en-2-yl)benzene

Guidance literature:: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine; In tetrahydrofuran; at 50 ℃; for 2h; further Pd catalyst;
DOI:10.1016/0040-4039(90)87025-U

Reference yield: 83.0%

: 1020852-36-1
tert-butyl ((S)-2-hydroxy-3-phenylpropionylamino)acetate

: 86537-63-5
Ethyl 2-Phenyl-2-propenyl carbonate

: tert-butyl (R)-2-((S)-2-hydroxy-3-phenylpropanamido)-4-phenylpent-4-enoate

Guidance literature:: tert-butyl ((S)-2-hydroxy-3-phenylpropionylamino)acetate; With triisopropoxytitanium(IV) chloride; In tetrahydrofuran; hexane; at 20 ℃; for 0.333333h; Schlenk technique;

With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; Schlenk technique;

Ethyl 2-Phenyl-2-propenyl carbonate; With bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In tetrahydrofuran; at -78 - 20 ℃; stereoselective reaction; Schlenk technique;
DOI:10.1021/acs.orglett.9b01497