dimethyl 2,5-dimethyl-1H-pyrrole-3,4-dicarboxylate

Base Information

Chemical Name:dimethyl 2,5-dimethyl-1H-pyrrole-3,4-dicarboxylate
CAS No.:40801-09-0
Molecular Formula:C10H13 N O4
Molecular Weight:211.218
Hs Code.:
Mol file:40801-09-0.mol

Synonyms:1H-Pyrrole-3,4-dicarboxylicacid, 2,5-dimethyl-, dimethyl ester (9CI);Pyrrole-3,4-dicarboxylic acid, 2,5-dimethyl-, dimethylester (7CI); NSC 225258

Suppliers and Price of dimethyl 2,5-dimethyl-1H-pyrrole-3,4-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 5 raw suppliers

Chemical Property of dimethyl 2,5-dimethyl-1H-pyrrole-3,4-dicarboxylate

Chemical Property:

Vapor Pressure:1.43E-05mmHg at 25°C
Boiling Point:366.7°Cat760mmHg
Flash Point:175.6°C
Density:1.199g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of dimethyl 2,5-dimethyl-1H-pyrrole-3,4-dicarboxylate

There total 4 articles about dimethyl 2,5-dimethyl-1H-pyrrole-3,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 27126-76-7
[hydroxy(tosyloxy)iodo]benzene

: 21731-17-9
methyl 3-aminocrotonate

: 40801-09-0
2,5-dimethyl-1H-pyrrole-3,4-dicarboxylic acid dimethyl ester

: methyl 2-iodo-2-tosyloxy-3-ketobutanoate

: methyl E-2-tosyloxy-3-aminocrotonate

: methyl E-2-phenyliodonio-3-amino-crotonate tosylate

Guidance literature:: In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/S0040-4020(97)10354-4

Reference yield: 70.0%

: 21731-17-9
methyl 3-aminocrotonate

: 90788-30-0
ethyl (Z)-3-(ethylamino)-3-phenylacrylate

: 3-ethyl 4-methyl 1-ethyl-5-methyl-2-phenyl-1H-pyrrole-3,4-dicarboxylate

: 40801-09-0
2,5-dimethyl-1H-pyrrole-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: With 2,2,2-trifluoroethanol; lithium perchlorate; In acetonitrile; at 20 ℃; for 2.5h; chemoselective reaction; Electrochemical reaction;
DOI:10.1002/anie.202111679

Reference yield: 69.0%

: ethyl (Z)-3-amino-3-(3,4-dimethylphenyl)acrylate

: 21731-17-9
methyl 3-aminocrotonate

: C₂₆H₂₉NO₄

: 3-ethyl 4-methyl 2-(3,4-dimethylphenyl)-5-methyl-1H-pyrrole-3,4-dicarboxylate

: 40801-09-0
2,5-dimethyl-1H-pyrrole-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: With 2,2,2-trifluoroethanol; lithium perchlorate; In acetonitrile; at 20 ℃; for 2.5h; chemoselective reaction; Electrochemical reaction;
DOI:10.1002/anie.202111679