2-BENZYLOXY-N-METHOXY-N-METHYL-BENZAMIDE

Base Information

• Chemical Name: 2-BENZYLOXY-N-METHOXY-N-METHYL-BENZAMIDE
• CAS No.: 873556-56-0
• Molecular Formula: C16H17NO3
• Molecular Weight: 271.316
• Hs Code.: 2924299090
• Mol file: 873556-56-0.mol

Synonyms:2-Benzyloxy-N-methoxy-N-methyl;2-BENZYLOXY-N-METHOXY-N-METHYL-BENZAMIDE;

Chemical Property of 2-BENZYLOXY-N-METHOXY-N-METHYL-BENZAMIDE

Chemical Property:

• PSA: 38.77000
• LogP: 2.89900

Purity/Quality:

99% ^*data from raw suppliers

2-Benzyloxy-N-methoxy-N-methylbenzamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-BENZYLOXY-N-METHOXY-N-METHYL-BENZAMIDE

There total 3 articles about 2-BENZYLOXY-N-METHOXY-N-METHYL-BENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-benzyloxybenzoyl chloride (4349-62-6) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → 2-(benzyloxy)-N-methoxy-N-methylbenzamide (873556-56-0)

Guidance literature:

With triethylamine; In chloroform; at 20 ℃; for 2.5h;

DOI:10.1021/jm051060o

Reference yield:

2-benzyloxybenzoic acid (14389-86-7) + N,O-dimethylhydroxylamine*hydrochloride (6638-79-5) → 2-(benzyloxy)-N-methoxy-N-methylbenzamide (873556-56-0)

Guidance literature:

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1016/j.tetlet.2011.03.018

Reference yield:

2-benzyloxybenzoic acid (14389-86-7) → 2-(benzyloxy)-N-methoxy-N-methylbenzamide (873556-56-0)

Guidance literature:

Multi-step reaction with 2 steps

1: (COCl)2; DMF / CH₂Cl₂ / 2 h

2: 1.19 g / Et₃N / CHCl₃ / 2.5 h / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; chloroform;

DOI:10.1021/jm051060o

upstream raw materials:

2-benzyloxybenzoyl chloride

N,O-dimethylhydroxylamine*hydrochloride

2-benzyloxybenzoic acid

Downstream raw materials:

1-(2-benzyloxy)phenyl-3-(trimethylsilyl)prop-2-yn-1-one

1-(2-(benzyloxy)phenyl)hex-2-yn-1-one

1-(2-(benzyloxy)phenyl)-3-(4-methoxyphenyl)prop-2-yn-1-one

N⁶-tert-butoxycarbonyl-5'-N-(4-(2-benzyloxybenzoyl)-1H-1,2,3-triazol-1-yl)-5'-deoxy-2',3'-O-isopropylideneadenosine

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