N-Piperonylidene-P-anisidine

Base Information

• Chemical Name: N-Piperonylidene-P-anisidine
• CAS No.: 24033-09-8
• Molecular Formula: C15H13 N O3
• Molecular Weight: 255.273
• European Community (EC) Number: 667-107-8
• NSC Number: 127719
• Nikkaji Number: J2.057.732K,J2.168.364G
• Mol file: 24033-09-8.mol

Synonyms:NSC127719;SCHEMBL4231715;SCHEMBL4231718;SCHEMBL20871099;N-PIPERONYLIDENE-P-ANISIDINE;AKOS024335186;NSC-127719;24033-09-8

Chemical Property of N-Piperonylidene-P-anisidine

Chemical Property:

• Vapor Pressure: 1.12E-06mmHg at 25°C
• Boiling Point: 413.8°Cat760mmHg
• Flash Point: 164.6°C
• Density: 1.2g/cm³
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 255.08954328
• Heavy Atom Count: 19
• Complexity: 313

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)N=CC2=CC3=C(C=C2)OCO3

Technology Process of N-Piperonylidene-P-anisidine

There total 7 articles about N-Piperonylidene-P-anisidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

→ N-(benzo[d][1,3]dioxol-5-ylmethylene)-4-methoxyaniline (24033-09-8)

Guidance literature:

Reference yield: 93.0%

piperonol (495-76-1) + 4-methoxy-aniline (104-94-9) → N-(benzo[d][1,3]dioxol-5-ylmethylene)-4-methoxyaniline (24033-09-8)

Guidance literature:

With C₃₄H₃₈Cl₂N₂O₂Ru₂; potassium tert-butylate; In tetrahydrofuran; at 25 - 30 ℃; for 24h; Molecular sieve;

DOI:10.1002/ejoc.201701408

Reference yield: 87.0%

piperonal (120-57-0,30024-74-9) + 4-methoxy-aniline (104-94-9) → N-(benzo[d][1,3]dioxol-5-ylmethylene)-4-methoxyaniline (24033-09-8)

Guidance literature:

With magnesium sulfate; In dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/jm9803323

upstream raw materials:

piperonal

4-methoxy-aniline

methanol

aniline

Downstream raw materials:

1-(p-methoxyphenyl)-3-phenyl-4-(3',4'-methylenedioxyphenyl)-azetidin-2-one

1-(p-methoxyphenyl)-3-(2',4'-dichlorophenoxy)-4-(3',4'-methylenedioxyphenyl)-azetidin-2-one

1-(p-methoxyphenyl)-3-ethoxy-4-(3',4'-methylenedioxyphenyl)-azetidin-2-one

1-p-Anisyl-3-carbethoxyacetonylamino-4-(3,4-methylenedioxyphenyl)azetidin-2-one