Carbonic acid, 4-[(2S)-3-[[4-[[[(4-nitrophenoxy)carbonyl]oxy]methyl]phenyl]amino]-3-oxo -2-[[(2-propenyloxy)carbonyl]amino]propyl]phenyl 2-propenyl ester

Base Information

Chemical Name:Carbonic acid, 4-[(2S)-3-[[4-[[[(4-nitrophenoxy)carbonyl]oxy]methyl]phenyl]amino]-3-oxo -2-[[(2-propenyloxy)carbonyl]amino]propyl]phenyl 2-propenyl ester
CAS No.:875153-71-2
Molecular Formula:C31H29N3O11
Molecular Weight:619.585
Hs Code.:

Carbonic acid,
4-[(2S)-3-[[4-[[[(4-nitrophenoxy)carbonyl]oxy]methyl]phenyl]amino]-3-oxo
-2-[[(2-propenyloxy)carbonyl]amino]propyl]phenyl 2-propenyl ester

Synonyms:

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Chemical Property of Carbonic acid, 4-[(2S)-3-[[4-[[[(4-nitrophenoxy)carbonyl]oxy]methyl]phenyl]amino]-3-oxo -2-[[(2-propenyloxy)carbonyl]amino]propyl]phenyl 2-propenyl ester

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Technology Process of Carbonic acid, 4-[(2S)-3-[[4-[[[(4-nitrophenoxy)carbonyl]oxy]methyl]phenyl]amino]-3-oxo -2-[[(2-propenyloxy)carbonyl]amino]propyl]phenyl 2-propenyl ester

There total 3 articles about Carbonic acid, 4-[(2S)-3-[[4-[[[(4-nitrophenoxy)carbonyl]oxy]methyl]phenyl]amino]-3-oxo -2-[[(2-propenyloxy)carbonyl]amino]propyl]phenyl 2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 728916-20-9
Carbonic acid allyl ester 4-[(S)-2-allyloxycarbonylamino-2-(4-hydroxymethyl-phenylcarbamoyl)-ethyl]-phenyl ester

: 875153-71-2
C₃₁H₂₉N₃O₁₁

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmcl.2004.04.041

Reference yield:

: 623-04-1
4-aminobenzenemethanol

: 875153-71-2
C₃₁H₂₉N₃O₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / EDCI; HOBt / tetrahydrofuran / 12 h / 20 °C

2: 98.8 percent / pyridine / tetrahydrofuran / 12 h / 20 °C

With pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2005.08.015

Reference yield:

: 104669-68-3
N,O-bis-allyloxycarbonyl-L-tyrosine

: 875153-71-2
C₃₁H₂₉N₃O₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / EDCI; HOBt / tetrahydrofuran / 12 h / 20 °C

2: 98.8 percent / pyridine / tetrahydrofuran / 12 h / 20 °C

With pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2005.08.015