Phenyl 2-(benzylamino)-1-bromoethane-1-sulfonate

Base Information

Chemical Name:Phenyl 2-(benzylamino)-1-bromoethane-1-sulfonate
CAS No.:87975-13-1
Molecular Formula:C15H16BrNO3S
Molecular Weight:370.267
Hs Code.:
DSSTox Substance ID:DTXSID50579397

Synonyms:Phenyl 2-(benzylamino)-1-bromoethane-1-sulfonate;87975-13-1;DTXSID50579397

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl 2-(benzylamino)-1-bromoethane-1-sulfonate

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:369.00343
Heavy Atom Count:21
Complexity:384

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)CNCC(S(=O)(=O)OC2=CC=CC=C2)Br

Technology Process of Phenyl 2-(benzylamino)-1-bromoethane-1-sulfonate

There total 4 articles about Phenyl 2-(benzylamino)-1-bromoethane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 6904-89-8
Phenyl 1-bromoethenesulfonate

: 100-46-9
benzylamine

: 87975-13-1
1-Bromo-1-phenoxysulfonyl-2-benzylaminoethane

Guidance literature:: In benzene; for 24h; Ambient temperature;
DOI:10.1055/s-1983-30527

Reference yield: 41.0%

: 6855-00-1
Phenyl 1,2-dibromoethanesulfonate

: 100-46-9
benzylamine

: 87975-13-1
1-Bromo-1-phenoxysulfonyl-2-benzylaminoethane

Guidance literature:: In benzene; for 24h; Ambient temperature;
DOI:10.1055/s-1983-30527

Reference yield:

: 1562-34-1
phenyl vinylsulfonate

: 87975-13-1
1-Bromo-1-phenoxysulfonyl-2-benzylaminoethane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Br₂, azodiisobutyronitrile / CCl₄ / 1.) reflux, 4 h; 2,) room temp., 48 h

2: 80 percent / triethylamine / benzene / 24 h / Ambient temperature

3: 41 percent / benzene / 24 h / Ambient temperature

With 2,2'-azobis(isobutyronitrile); bromine; triethylamine; In tetrachloromethane; benzene;
DOI:10.1055/s-1983-30527