4-[[4-Chloro-1-(2,4-dimethoxyphenyl)-2,5-dioxopyrrol-3-yl]amino]benzoate

Base Information

Chemical Name:4-[[4-Chloro-1-(2,4-dimethoxyphenyl)-2,5-dioxopyrrol-3-yl]amino]benzoate
CAS No.:6904-89-8
Molecular Formula:C19H14ClN2O6-
Molecular Weight:401.7778
Hs Code.:
DSSTox Substance ID:DTXSID30364809
Wikidata:Q82148972

Synonyms:6904-89-8;DTXSID30364809;4-[[4-chloro-1-(2,4-dimethoxyphenyl)-2,5-dioxopyrrol-3-yl]amino]benzoate

Suppliers and Price of 4-[[4-Chloro-1-(2,4-dimethoxyphenyl)-2,5-dioxopyrrol-3-yl]amino]benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[[4-Chloro-1-(2,4-dimethoxyphenyl)-2,5-dioxopyrrol-3-yl]amino]benzoate

Chemical Property:

Vapor Pressure:1.63E-14mmHg at 25°C
Boiling Point:584.7°C at 760 mmHg
Flash Point:307.4°C
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:401.0540389
Heavy Atom Count:28
Complexity:668

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)N2C(=O)C(=C(C2=O)Cl)NC3=CC=C(C=C3)C(=O)[O-])OC

Technology Process of 4-[[4-Chloro-1-(2,4-dimethoxyphenyl)-2,5-dioxopyrrol-3-yl]amino]benzoate

There total 2 articles about 4-[[4-Chloro-1-(2,4-dimethoxyphenyl)-2,5-dioxopyrrol-3-yl]amino]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6855-00-1
Phenyl 1,2-dibromoethanesulfonate

: 6904-89-8
Phenyl 1-bromoethenesulfonate

Guidance literature:: With triethylamine; In benzene; for 24h; Ambient temperature;
DOI:10.1055/s-1983-30527

Reference yield:

: 1562-34-1
phenyl vinylsulfonate

: 6904-89-8
Phenyl 1-bromoethenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Br₂, azodiisobutyronitrile / CCl₄ / 1.) reflux, 4 h; 2,) room temp., 48 h

2: 80 percent / triethylamine / benzene / 24 h / Ambient temperature

With 2,2'-azobis(isobutyronitrile); bromine; triethylamine; In tetrachloromethane; benzene;
DOI:10.1055/s-1983-30527