6-Chloro-4-(2-chlorophenyl)-3-oxo-1,2,3lambda~5~-benzotriazine

Base Information

Chemical Name:6-Chloro-4-(2-chlorophenyl)-3-oxo-1,2,3lambda~5~-benzotriazine
CAS No.:87999-67-5
Molecular Formula:C13H7Cl2N3O
Molecular Weight:292.124
Hs Code.:
DSSTox Substance ID:DTXSID80520130
Wikidata:Q82383814

Synonyms:87999-67-5;DTXSID80520130;6-Chloro-4-(2-chlorophenyl)-3-oxo-1,2,3lambda~5~-benzotriazine

Suppliers and Price of 6-Chloro-4-(2-chlorophenyl)-3-oxo-1,2,3lambda~5~-benzotriazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 6-Chloro-4-(2-chlorophenyl)-3-oxo-1,2,3lambda~5~-benzotriazine

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:290.9966172
Heavy Atom Count:19
Complexity:320

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C2=[N+](N=NC3=C2C=C(C=C3)Cl)[O-])Cl

Technology Process of 6-Chloro-4-(2-chlorophenyl)-3-oxo-1,2,3lambda~5~-benzotriazine

There total 3 articles about 6-Chloro-4-(2-chlorophenyl)-3-oxo-1,2,3lambda~5~-benzotriazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 13949-49-0
2',5-Dichloro-2-aminobenzophenone oxime

: 87999-67-5
6-Chloro-4-(o-chlorophenyl)-1,2,3-benzotriazine 3-Oxide

Guidance literature:: With hydrogenchloride; sodium nitrite; In ethanol; water; for 0.25h; ice bath;
DOI:10.1021/jo00176a015

Reference yield:

: 2958-36-3,53960-29-5
(2-amino-5-chloro-phenyl)-(2-chloro-phenyl)-methanone

: 87999-67-5
6-Chloro-4-(o-chlorophenyl)-1,2,3-benzotriazine 3-Oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaNO₂/HCl/aq. CH₃COOH, 2) aq. KI

2: 27.4 percent / NH₂OH*HCl, piperidine / pyridine / 20 h / Heating

3: 83 percent / NaNO₂, 1 N HCl / ethanol; H₂O / 0.25 h / ice bath

With piperidine; hydrogenchloride; hydroxylamine hydrochloride; acetic acid; potassium iodide; sodium nitrite; In pyridine; ethanol; water;
DOI:10.1021/jo00176a015

Reference yield:

: 76049-50-8
2',5-dichloro-2-iodobenzophenone

: 87999-67-5
6-Chloro-4-(o-chlorophenyl)-1,2,3-benzotriazine 3-Oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 27.4 percent / NH₂OH*HCl, piperidine / pyridine / 20 h / Heating

2: 83 percent / NaNO₂, 1 N HCl / ethanol; H₂O / 0.25 h / ice bath

With piperidine; hydrogenchloride; hydroxylamine hydrochloride; sodium nitrite; In pyridine; ethanol; water;
DOI:10.1021/jo00176a015