1-(Dimethoxymethyl)-3-nitrobenzene

Base Information

Chemical Name:1-(Dimethoxymethyl)-3-nitrobenzene
CAS No.:3395-79-7
Molecular Formula:C9H11 N O4
Molecular Weight:197.191
Hs Code.:2909309090
European Community (EC) Number:663-149-6
NSC Number:105562
DSSTox Substance ID:DTXSID80295795
Nikkaji Number:J406.168C
Wikidata:Q82035959
Mol file:3395-79-7.mol

Synonyms:1-(dimethoxymethyl)-3-nitrobenzene;3395-79-7;3-Nitrobenzaldehydedimethylacetal;NSC105562;NCIOpen2_002117;SCHEMBL7700608;DTXSID80295795;3-Nitrobenzaldehyde dimethylacetal;ALXDDWGEZDTXOE-UHFFFAOYSA-N;m-nitro-benzaldehyde dimethyl acetal;STL453675;1-(dimethoxy-methyl)-3-nitro-benzene;AKOS006281040;NSC-105562;Benzene, 1-(dimethoxymethyl)-3-nitro-;FT-0657925

Suppliers and Price of 1-(Dimethoxymethyl)-3-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
m-NitrobenzaldehydeDimethylAcetal
5g
$ 175.00

Sigma-Aldrich
3-NITROBENZALDEHYDE DIMETHYL ACETAL AldrichCPR
1g
$ 32.30

American Custom Chemicals Corporation
3-NITROBENZALDEHYDE DIMETHYL ACETAL 95.00%
1G
$ 727.65

Total 2 raw suppliers

Chemical Property of 1-(Dimethoxymethyl)-3-nitrobenzene

Chemical Property:

Vapor Pressure:0.0471mmHg at 25°C
Melting Point:24°C (estimate)
Refractive Index:1.5310 (estimate)
Boiling Point:244.6°Cat760mmHg
Flash Point:96°C
PSA：64.28000
Density:1.201g/cm³
LogP:2.40940
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:197.06880783
Heavy Atom Count:14
Complexity:188

Purity/Quality:

97% ^*data from raw suppliers

m-NitrobenzaldehydeDimethylAcetal ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(C1=CC(=CC=C1)[N+](=O)[O-])OC

Technology Process of 1-(Dimethoxymethyl)-3-nitrobenzene

There total 9 articles about 1-(Dimethoxymethyl)-3-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 67-56-1
methanol

: 99-61-6
3-nitro-benzaldehyde

: 3395-79-7
m-nitrobenzaldehyde dimethylacetal

Guidance literature:: With phosphoric acid functionalized ethanolamine grafted polyacrylonitrile fiber; at 65 ℃; for 3.5h; Green chemistry;
DOI:10.1002/asia.201700846

Reference yield: 59.0%

: 431-47-0
trifluoroacetic acid-methyl ester

: 124-41-4
sodium methylate

: 99-61-6
3-nitro-benzaldehyde

: 3395-79-7
m-nitrobenzaldehyde dimethylacetal

Guidance literature:: In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1039/c8ob00017d

Reference yield:

: 67-56-1
methanol

: 586-39-0,51209-60-0
1-nitro-3-vinyl-benzene

: 3395-79-7
m-nitrobenzaldehyde dimethylacetal

: 99-61-6
3-nitro-benzaldehyde

Guidance literature:: With 2-Picolinic acid; ferrous(II) sulfate heptahydrate; dihydrogen peroxide; at 20 - 60 ℃; for 12h; Schlenk technique; Molecular sieve;
DOI:10.1002/cctc.201300270