2-Chloro-N-(2-sulfanylidene-1,2-dihydropyridin-3-yl)benzamide

Base Information

Chemical Name:2-Chloro-N-(2-sulfanylidene-1,2-dihydropyridin-3-yl)benzamide
CAS No.:88369-28-2
Molecular Formula:C₁₂H₉ClN₂OS
Molecular Weight:264.735
Hs Code.:
DSSTox Substance ID:DTXSID30521551
Wikidata:Q82386087

Synonyms:88369-28-2;DTXSID30521551;2-Chloro-N-(2-sulfanylidene-1,2-dihydropyridin-3-yl)benzamide

Suppliers and Price of 2-Chloro-N-(2-sulfanylidene-1,2-dihydropyridin-3-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Chloro-N-(2-sulfanylidene-1,2-dihydropyridin-3-yl)benzamide

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:264.0124118
Heavy Atom Count:17
Complexity:392

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NC2=CC=CNC2=S)Cl

Technology Process of 2-Chloro-N-(2-sulfanylidene-1,2-dihydropyridin-3-yl)benzamide

There total 4 articles about 2-Chloro-N-(2-sulfanylidene-1,2-dihydropyridin-3-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52334-72-2
3-(2'-chlorobenzoyl)aminopyrid-2-one

: 88369-28-2
3-(2'-chlorobenzoyl)aminothiopyrid-2-one

Guidance literature:: With tetraphosphorus decasulfide; In pyridine; raised from 20 deg C to 60 deg C in 0.5 h, then 3.5 h at 60 deg C;
DOI:10.1002/jhet.5570200535

Reference yield:

: 6298-19-7
2-chloro-3-aminopyridine

: 88369-28-2
3-(2'-chlorobenzoyl)aminothiopyrid-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / toluene / 1 h / Heating

2: 89 percent / NH₄Cl, polyphosphoric acid / 12 h / 180 °C

3: P₂S₅ / pyridine / raised from 20 deg C to 60 deg C in 0.5 h, then 3.5 h at 60 deg C

With pyridine; PPA; tetraphosphorus decasulfide; ammonium chloride; In pyridine; toluene;
DOI:10.1002/jhet.5570200535

Reference yield:

: 84446-21-9
3-(2'-chlorobenzoyl)amino-2-chloropyridine

: 88369-28-2
3-(2'-chlorobenzoyl)aminothiopyrid-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NH₄Cl, polyphosphoric acid / 12 h / 180 °C

2: P₂S₅ / pyridine / raised from 20 deg C to 60 deg C in 0.5 h, then 3.5 h at 60 deg C

With PPA; tetraphosphorus decasulfide; ammonium chloride; In pyridine;
DOI:10.1002/jhet.5570200535