BENZYL N-STYRYLCARBAMATE

Base Information

• Chemical Name: BENZYL N-STYRYLCARBAMATE
• CAS No.: 88425-24-5
• Molecular Formula: C16H15NO2
• Molecular Weight: 253.301
• Mol file: 88425-24-5.mol

Synonyms:styrylcarbamic acid benzyl ester;N-(benzyloxycarbonyl)-1-amino-trans-styrene;BENZYL-N-STYRYLCARBAMATE;(E)-benzyl styrylcarbamate;benzyl styrylcarbamate;

Chemical Property of BENZYL N-STYRYLCARBAMATE

Chemical Property:

• PSA: 38.33000
• LogP: 3.97460

Purity/Quality:

BENZYL-N-STYRYLCARBAMATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL N-STYRYLCARBAMATE

There total 13 articles about BENZYL N-STYRYLCARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(E)-cinnamoyl azide (26829-64-1) + benzyl alcohol (100-51-6,185532-71-2) → N-benzyloxycarbonylamino-2-phenyl-(E)-ethylene (88425-24-5)

Guidance literature:

With pyridine; hydroquinone; In toluene; at 100 ℃; for 0.5h;

DOI:10.1039/c7ob01766a

Reference yield: 87.0%

benzyloxycarbonyl azide (3422-03-5) + trans-2-phenylvinylboronic acid (6783-05-7) → N-benzyloxycarbonylamino-2-phenyl-(E)-ethylene (88425-24-5)

Guidance literature:

With copper(l) chloride; In methanol; at 20 ℃; for 2h;

DOI:10.1021/jo502828r

Reference yield: 59.0%

S-pyridin-2-yl 2-(((benzyloxy)carbonyl)amino)-3-phenylpropanethioate (33861-71-1) → (Z)-benzyl styrylcarbamate (1251840-96-6) + N-benzyloxycarbonylamino-2-phenyl-(E)-ethylene (88425-24-5)

Guidance literature:

With bis(η3-allyl-μ-chloropalladium(II)); N-ethyl-N,N-diisopropylamine; catacxium A; In 1,4-dioxane; at 105 ℃; for 18h;

DOI:10.1021/ol101620r

upstream raw materials:

methanol

N-(Benzyloxycarbonyl)-N'-carbonyl-1,1-diamino-2-phenylethane

(E)-3-phenylacrylic acid

benzyl chloroformate