Benzamide, N,N-diethyl-2-methoxy-6-methyl-

Base Information

Chemical Name:Benzamide, N,N-diethyl-2-methoxy-6-methyl-
CAS No.:88430-97-1
Molecular Formula:C13H19NO2
Molecular Weight:221.299
Hs Code.:
DSSTox Substance ID:DTXSID00446106
Nikkaji Number:J314.940D
Wikidata:Q82264684

Synonyms:Benzamide, N,N-diethyl-2-methoxy-6-methyl-;88430-97-1;DTXSID00446106;N,N-Diethyl-2-methoxy-6-methylbenzamide

Suppliers and Price of Benzamide, N,N-diethyl-2-methoxy-6-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzamide, N,N-diethyl-2-methoxy-6-methyl-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:221.141578849
Heavy Atom Count:16
Complexity:226

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C=CC=C1OC)C

Technology Process of Benzamide, N,N-diethyl-2-methoxy-6-methyl-

There total 10 articles about Benzamide, N,N-diethyl-2-methoxy-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 594-27-4
tetramethylstannane

: 154045-66-6
2-diethylcarbamoyl-3-methoxyphenyl trifluoromethanesulfonate

: 88430-97-1
N,N-diethyl-2-methoxy-6-methylbenzamide

Guidance literature:: With triphenylphosphine; lithium chloride; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 120 ℃; for 8h;
DOI:10.1016/S0040-4039(00)73902-5

Reference yield:

: 85630-30-4
N,N-diethyl-2-hydroxy-6-methoxybenzamide

: 88430-97-1
N,N-diethyl-2-methoxy-6-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 49 percent / LiCl, PPh₃, PdCl₂(PPh₃)2 / dimethylformamide / 8 h / 120 °C

With bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride; In pyridine; N,N-dimethyl-formamide;

Reference yield:

: 154045-69-9
1,2-dimethoxy-3-(methoxymethoxy)benzene

: 88430-97-1
N,N-diethyl-2-methoxy-6-methylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: K / tetrahydrofuran / 1.) room temperature, 12-18 h, 2.) -40 deg C, 2.5 h

2: 0.6 mol dm^-3 HCl / methanol / 1 h / Ambient temperature

3: pyridine

4: 49 percent / LiCl, PPh₃, PdCl₂(PPh₃)2 / dimethylformamide / 8 h / 120 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium; triphenylphosphine; lithium chloride; In tetrahydrofuran; pyridine; methanol; N,N-dimethyl-formamide;