Technology Process of 1-Piperidinecarboxylic acid, 4-(phenylacetyl)-, 1,1-dimethylethyl ester
There total 9 articles about 1-Piperidinecarboxylic acid, 4-(phenylacetyl)-, 1,1-dimethylethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate;
In
acetonitrile;
at 20 ℃;
Inert atmosphere;
Irradiation;
DOI:10.1002/anie.202105354
- Guidance literature:
-
With
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide;
In
dichloromethane;
at 0 - 20 ℃;
for 15h;
Molecular sieve;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 12 h / 20 °C / Inert atmosphere
2: caesium carbonate; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; 1,4-dimethyl-1,2,4-triazolium iodide / acetonitrile / 20 °C / Inert atmosphere; Irradiation; Sealed tube
With
[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate; 1,4-dimethyl-1,2,4-triazolium iodide;
In
dichloromethane; acetonitrile;
DOI:10.1002/anie.202001824
