Ethanone, 1,1'-[1,3-propanediylbis(oxy-4,1-phenylene)]bis-

Base Information

• Chemical Name: Ethanone, 1,1'-[1,3-propanediylbis(oxy-4,1-phenylene)]bis-
• CAS No.: 88949-86-4
• Molecular Formula: C19H20O4
• Molecular Weight: 312.365
• DSSTox Substance ID: DTXSID50372421
• Nikkaji Number: J2.641.610H
• Wikidata: Q82160126
• Mol file: 88949-86-4.mol

Synonyms:Ethanone, 1,1'-[1,3-propanediylbis(oxy-4,1-phenylene)]bis-;88949-86-4;1-[4-[3-(4-acetylphenoxy)propoxy]phenyl]ethanone;Maybridge1_008099;HMS564I03;DTXSID50372421;YPQDOUIKXGJRCR-UHFFFAOYSA-N;CCG-47774;4',4'''-(Trimethylenebisoxy)bis(acetophenone);SR-01000637367-1;1,1'-[propane-1,3-diylbis(oxybenzene-4,1-diyl)]diethanone

Chemical Property of Ethanone, 1,1'-[1,3-propanediylbis(oxy-4,1-phenylene)]bis-

Chemical Property:

• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 8
• Exact Mass: 312.13615911
• Heavy Atom Count: 23
• Complexity: 341

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)C1=CC=C(C=C1)OCCCOC2=CC=C(C=C2)C(=O)C

Technology Process of Ethanone, 1,1'-[1,3-propanediylbis(oxy-4,1-phenylene)]bis-

There total 2 articles about Ethanone, 1,1'-[1,3-propanediylbis(oxy-4,1-phenylene)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,3-dibromo-propane (109-64-8) + 4-hydroxy-benzoic acid (99-96-7) → 1,1'-<1,3-propanediylbis(oxy-4,1-phenylene)>bisethanone (88949-86-4)

Guidance literature:

With potassium carbonate; at 115 - 130 ℃; for 2h;

DOI:10.1021/jm801006v

Reference yield: 90.0%

1,3-dibromo-propane (109-64-8) + 4-Hydroxyacetophenone (99-93-4) → 1,1'-<1,3-propanediylbis(oxy-4,1-phenylene)>bisethanone (88949-86-4)

Guidance literature:

With potassium carbonate; In acetone; Reflux;

DOI:10.3109/14756366.2015.1021253

Reference yield: 95.0%

1,1'-<1,3-propanediylbis(oxy-4,1-phenylene)>bisethanone (88949-86-4) + 4-methoxy-benzaldehyde (123-11-5) → C35H32O6

Guidance literature:

With sodium hydroxide; In ethanol; at 20 ℃;

DOI:10.1002/jhet.5570450547

upstream raw materials:

1,3-dibromo-propane

4-Hydroxyacetophenone

4-hydroxy-benzoic acid

Downstream raw materials:

1,3-Bis-(4-ethinyl-phenoxy)-propan

N'-[1-[4-(3-{4-[1-(Ethoxycarbonyl-hydrazono)-ethyl]-phenoxy}-propoxy)-phenyl]-eth-(E)-ylidene]-hydrazinecarboxylic acid ethyl ester

(2E,2'E)-1,1'-((propane-1,3-diylbis(oxy))bis(4,1-phenylene))bis(3-phenylprop-2-en-1-one)

(E)-3-(3,4-Dimethoxy-phenyl)-1-[4-(3-{4-[(E)-3-(3,4-dimethoxy-phenyl)-acryloyl]-phenoxy}-propoxy)-phenyl]-propenone