Benzeneacetic acid, a-methyl-2-(methyl-2-thiazolylamino)-

Base Information

Chemical Name:Benzeneacetic acid, a-methyl-2-(methyl-2-thiazolylamino)-
CAS No.:88975-79-5
Molecular Formula:C₁₃H₁₄N₂O₂S
Molecular Weight:262.332
Hs Code.:

Synonyms:

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Chemical Property of Benzeneacetic acid, a-methyl-2-(methyl-2-thiazolylamino)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzeneacetic acid, a-methyl-2-(methyl-2-thiazolylamino)-

There total 10 articles about Benzeneacetic acid, a-methyl-2-(methyl-2-thiazolylamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65548-02-9
(+/-)-ethyl cyano(2-nitrophenyl)acetate

: 88975-79-5
2-<2-(N-methyl-N-thiazol-2-ylamino)phenyl>propionic acid

Guidance literature:: Multi-step reaction with 9 steps

1: 63.4 percent / K₂CO₃ / acetone / 5 h / Heating

2: 82.9 percent / K₂CO₃ / aq. ethanol / 18 h / Heating

3: 89.8 percent / H₂ / 5percent Pd-C / ethanol

4: 99.3 percent / CH₂Cl₂ / 1 h / Ambient temperature

5: 11.0 g / Na₂CO₃ / dimethylformamide / 2.5 h / Ambient temperature

6: 4.8percent aq. NaOH / benzene; dimethylformamide; H₂O / 1 h / 8 °C

7: 70 percent / NH₄SCN / acetone / 1 h / Ambient temperature

8: K₂CO₃ / methanol; H₂O / 9 h / Heating

9: p-toluenesulfonic acid / acetic acid / 8 h / 90 - 92 °C

With sodium hydroxide; hydrogen; ammonium thiocyanate; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1248/cpb.31.3424

Reference yield:

: 88-73-3
2-Chloronitrobenzene

: 88975-79-5
2-<2-(N-methyl-N-thiazol-2-ylamino)phenyl>propionic acid

Guidance literature:: Multi-step reaction with 10 steps

1: 98.6 g / NaH / dimethylformamide / 24 h / 44 - 47 °C

2: 63.4 percent / K₂CO₃ / acetone / 5 h / Heating

3: 82.9 percent / K₂CO₃ / aq. ethanol / 18 h / Heating

4: 89.8 percent / H₂ / 5percent Pd-C / ethanol

5: 99.3 percent / CH₂Cl₂ / 1 h / Ambient temperature

6: 11.0 g / Na₂CO₃ / dimethylformamide / 2.5 h / Ambient temperature

7: 4.8percent aq. NaOH / benzene; dimethylformamide; H₂O / 1 h / 8 °C

8: 70 percent / NH₄SCN / acetone / 1 h / Ambient temperature

9: K₂CO₃ / methanol; H₂O / 9 h / Heating

10: p-toluenesulfonic acid / acetic acid / 8 h / 90 - 92 °C

With sodium hydroxide; hydrogen; ammonium thiocyanate; sodium hydride; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1248/cpb.31.3424

Reference yield:

: 65783-00-8
2-(2-nitrophenyl)propanenitrile

: 88975-79-5
2-<2-(N-methyl-N-thiazol-2-ylamino)phenyl>propionic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 89.8 percent / H₂ / 5percent Pd-C / ethanol

2: 99.3 percent / CH₂Cl₂ / 1 h / Ambient temperature

3: 11.0 g / Na₂CO₃ / dimethylformamide / 2.5 h / Ambient temperature

4: 4.8percent aq. NaOH / benzene; dimethylformamide; H₂O / 1 h / 8 °C

5: 70 percent / NH₄SCN / acetone / 1 h / Ambient temperature

6: K₂CO₃ / methanol; H₂O / 9 h / Heating

7: p-toluenesulfonic acid / acetic acid / 8 h / 90 - 92 °C

With sodium hydroxide; hydrogen; ammonium thiocyanate; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1248/cpb.31.3424