N-Cyclohexyl-4-MethoxybenzaMide, 97%

Base Information

• Chemical Name: N-Cyclohexyl-4-MethoxybenzaMide, 97%
• CAS No.: 33739-91-2
• Molecular Formula: C14H19NO2
• Molecular Weight: 233.31
• Hs Code.: 2924299090
• Mol file: 33739-91-2.mol

Synonyms:4-methoxy-benzoic acid cyclohexylamide;N-Cyclohexyl-4-methoxy-benzamide;Anisyl-cyclohexylamid;4-Methoxy-benzoesaeure-cyclohexylamid;N-Cyclohexyl-p-methoxybenzamid;p-methoxy-N-cyclohexyl benzamide;

Chemical Property of N-Cyclohexyl-4-MethoxybenzaMide, 97%

Chemical Property:

• Vapor Pressure: 8.41E-07mmHg at 25°C
• Boiling Point: 406°Cat760mmHg
• Flash Point: 199.3°C
• PSA: 38.33000
• Density: 1.09g/cm³
• LogP: 3.14860

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Cyclohexyl-4-MethoxybenzaMide, 97%

There total 43 articles about N-Cyclohexyl-4-MethoxybenzaMide, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

cyclohexylamine (108-91-8,157973-60-9) + 4-methoxybenzoic acid (100-09-4) → N-cyclohexyl-4-methoxybenzamide (33739-91-2)

Guidance literature:

With Bromotrichloromethane; 4-(diphenylphosphino)-benzyltrimethylammonium bromide; triethylamine; In tetrahydrofuran; at 60 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.tet.2013.03.021

Reference yield: 97.0%

4-methoxy-benzaldehyde (123-11-5) + cyclohexanol (108-93-0) → N-cyclohexyl-4-methoxybenzamide (33739-91-2)

Guidance literature:

4-methoxy-benzaldehyde; With sodium azide; trifluorormethanesulfonic acid; acetic acid; at 40 ℃; for 2h;

cyclohexanol; With trifluorormethanesulfonic acid; at 90 ℃;

DOI:10.1016/j.tetlet.2016.08.069

Reference yield: 95.0%

terephthalic acid (100-21-0) + cyclohexylamine (108-91-8,157973-60-9) → N-cyclohexyl-4-methoxybenzamide (33739-91-2)

Guidance literature:

cyclohexylamine; With iodine; triphenylphosphine; In dichloromethane; at 0 ℃; Inert atmosphere;

terephthalic acid; In dichloromethane; at 0 ℃; Inert atmosphere;

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.25h; Inert atmosphere;

DOI:10.1039/c5ra03184b

upstream raw materials:

cyclohexyl chloride

4-methoxybenzonitrile

methoxybenzene

Cyclohexyl isocyanate

Downstream raw materials:

C₂₁H₂₅NO

C₂₁H₂₅NO

N-(1-(4-methoxyphenyl)pentyl)cyclohexanamine

N-(bis(4-methoxyphenyl)methylene)cyclohexanamine

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