N-Methoxy-2-[(4-methoxyphenyl)sulfanyl]benzamide

Base Information

• Chemical Name: N-Methoxy-2-[(4-methoxyphenyl)sulfanyl]benzamide
• CAS No.: 89114-61-4
• Molecular Formula: C15H15NO3S
• Molecular Weight: 289.355
• DSSTox Substance ID: DTXSID20553588
• Wikidata: Q82434210

Synonyms:89114-61-4;benzamide,n-methoxy-2-[(4-methoxyphenyl)thio]-;N-Methoxy-2-[(4-methoxyphenyl)sulfanyl]benzamide;DTXSID20553588

Chemical Property of N-Methoxy-2-[(4-methoxyphenyl)sulfanyl]benzamide

Chemical Property:

• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 289.07726451
• Heavy Atom Count: 20
• Complexity: 306

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)SC2=CC=CC=C2C(=O)NOC

Technology Process of N-Methoxy-2-[(4-methoxyphenyl)sulfanyl]benzamide

There total 2 articles about N-Methoxy-2-[(4-methoxyphenyl)sulfanyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-<(4-methoxyphenyl)thio>benzoic acid (19862-91-0) → O-Methyl-2-(4-methoxyphenylthio)benzohydroxamic acid (89114-61-4)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / benzene / 4 h / Heating

2: pyridine / 0.5 h

With pyridine; thionyl chloride; In benzene;

DOI:10.1016/S0040-4020(01)87717-6

Reference yield:

2-(4-Methoxyphenylthio)benzoyl chloride (43183-12-6) + N-methoxylamine hydrochloride (593-56-6) → O-Methyl-2-(4-methoxyphenylthio)benzohydroxamic acid (89114-61-4)

Guidance literature:

With pyridine; for 0.5h; Yield given;

DOI:10.1016/S0040-4020(01)87717-6

Reference yield: 85.0%

O-Methyl-2-(4-methoxyphenylthio)benzohydroxamic acid (89114-61-4) → 2-(4-Methoxy-phenylsulfanyl)-benzamide (89114-62-5)

Guidance literature:

With 9,10-Dicyanoanthracene; In benzene; for 2h; Irradiation; methanol;

DOI:10.1016/S0040-4039(00)94138-8

upstream raw materials:

2-(4-Methoxyphenylthio)benzoyl chloride

N-methoxylamine hydrochloride

2-<(4-methoxyphenyl)thio>benzoic acid

Downstream raw materials:

2-methoxy-9H-thioxanthen-9-one

2-(4-Methoxy-phenylsulfanyl)-benzamide

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