Benzeneacetamide, N-[2-(1-cyclohexen-1-yl)ethyl]-2-hydroxy-

Base Information

Chemical Name:Benzeneacetamide, N-[2-(1-cyclohexen-1-yl)ethyl]-2-hydroxy-
CAS No.:89240-67-5
Molecular Formula:C16H21NO2
Molecular Weight:259.348
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneacetamide, N-[2-(1-cyclohexen-1-yl)ethyl]-2-hydroxy-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzeneacetamide, N-[2-(1-cyclohexen-1-yl)ethyl]-2-hydroxy-

There total 1 articles about Benzeneacetamide, N-[2-(1-cyclohexen-1-yl)ethyl]-2-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3399-73-3
2-(1-cyclohexenyl)ethylamine

: 614-75-5
2-Hydroxyphenylacetic acid

: 89240-67-5
N-<2-(1-cyclohexen-1-yl)ethyl>-2-(2-hydroxyphenyl)acetamide

Guidance literature:: In xylene; for 6h; Heating;
DOI:10.1002/hlca.19830660807

Reference yield: 88.0%

: 100-44-7
benzyl chloride

: 89240-67-5
N-<2-(1-cyclohexen-1-yl)ethyl>-2-(2-hydroxyphenyl)acetamide

: 89240-68-6
2-(2-benzyloxyphenyl)-N-<2-(1-cyclohexen-1-yl)ethyl>acetamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 3h;
DOI:10.1002/hlca.19830660807

Reference yield:

: 89240-67-5
N-<2-(1-cyclohexen-1-yl)ethyl>-2-(2-hydroxyphenyl)acetamide

: 1-(2-hydroxybenzyl)-N-methyl-1,2,3,4,5,6,7,8-octahydroisoquinoline hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / K₂CO₃ / dimethylformamide / 3 h / 85 °C

2: 11.5 g / POCl₃ / acetonitrile / 2 h / Heating

3: 10.3 g / NaBH₄ / ethanol / 10 deg C --> r.t.

4: 77 percent / NaOAc, 37percent formalin, 2N AcOH, H₂ / 10percent Pd/C / 16 h / 1551.4 Torr / Ambient temperature

With sodium tetrahydroborate; formaldehyd; hydrogen; sodium acetate; potassium carbonate; acetic acid; trichlorophosphate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/hlca.19830660807