3-(Diphenylphosphoryl)cyclohexan-1-one

Base Information

Chemical Name:3-(Diphenylphosphoryl)cyclohexan-1-one
CAS No.:89358-47-4
Molecular Formula:C18H19O2P
Molecular Weight:298.321
Hs Code.:
DSSTox Substance ID:DTXSID20527183
Nikkaji Number:J2.500.352G

Synonyms:89358-47-4;3-(Diphenylphosphoryl)cyclohexanone;3-(Diphenylphosphoryl)cyclohexan-1-one;DTXSID20527183

Suppliers and Price of 3-(Diphenylphosphoryl)cyclohexan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(Diphenylphosphoryl)cyclohexan-1-one

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:298.11226684
Heavy Atom Count:21
Complexity:383

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(CC(=O)C1)P(=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 3-(Diphenylphosphoryl)cyclohexan-1-one

There total 10 articles about 3-(Diphenylphosphoryl)cyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 930-68-7
cyclohexenone

: 678187-53-6
(tert-butyldimethylsilyl)diphenylphosphine

: 89358-47-4
3-(diphenylphosphoryl)cyclohexan-1-one

Guidance literature:: cyclohexenone; (tert-butyldimethylsilyl)diphenylphosphine; With Pd(2-PyCH=NPh)(OCOC₆F₅)2; In 1,4-dioxane; water; at 60 ℃; for 16h; Inert atmosphere;

With dihydrogen peroxide; In 1,4-dioxane; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol8028466

Reference yield: 84.0%

: 930-68-7
cyclohexenone

: 829-85-6
diphenylphosphane

: 89358-47-4
3-(diphenylphosphoryl)cyclohexan-1-one

Guidance literature:: With vanadyl triflate; at 20 ℃; for 21h;
DOI:10.1021/ol702302y

Reference yield: 81.0%

: 930-68-7
cyclohexenone

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 89358-47-4
3-(diphenylphosphoryl)cyclohexan-1-one

Guidance literature:: cyclohexenone; chloro-diphenylphosphine; With acetic acid; at 20 ℃; Inert atmosphere;

With water; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2011.09.093