2,6-Nonadien-1-ol, 9-(3,3-dimethyloxiranyl)-3,7-dimethyl-, benzoate

Base Information

Chemical Name:2,6-Nonadien-1-ol, 9-(3,3-dimethyloxiranyl)-3,7-dimethyl-, benzoate
CAS No.:89637-68-3
Molecular Formula:C22H30O3
Molecular Weight:342.478
Hs Code.:

Synonyms:10,11-epoxyfarnesyl benzoate;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-Nonadien-1-ol, 9-(3,3-dimethyloxiranyl)-3,7-dimethyl-, benzoate

Chemical Property:

Boiling Point:448.2±33.0 °C(Predicted)
PSA：70.06000
Density:1.013±0.06 g/cm3(Predicted)
LogP:4.99390

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,6-Nonadien-1-ol, 9-(3,3-dimethyloxiranyl)-3,7-dimethyl-, benzoate

There total 3 articles about 2,6-Nonadien-1-ol, 9-(3,3-dimethyloxiranyl)-3,7-dimethyl-, benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 89637-63-8
farnesyl benzoate

: 89637-68-3
10,11-epoxyfarnesyl benzoate

Guidance literature:: With N-Bromosuccinimide; In tetrahydrofuran; water; at 0 - 20 ℃; for 4h;

Reference yield: 26.0%

: 89637-63-8
farnesyl benzoate

: C₂₂H₃₀O₃

: 89637-68-3
10,11-epoxyfarnesyl benzoate

: C₂₂H₃₀O₄

Guidance literature:: With borax; Oxone; Shi's ketone; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; In Dimethoxymethane; water; acetonitrile; at 0 ℃; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo901920d

Reference yield:

: 4602-84-0
farnesol

: 98-88-4
benzoyl chloride

: 89637-68-3
10,11-epoxyfarnesyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h / 0 - 20 °C

2: N-Bromosuccinimide / tetrahydrofuran; water / 4 h / 0 - 20 °C

With pyridine; N-Bromosuccinimide; In tetrahydrofuran; water;