1-{4-[3-(4-Methoxyphenyl)acryloyl]phenyl}triaza-1,2-dien-2-ium

Base Information

Chemical Name:1-{4-[3-(4-Methoxyphenyl)acryloyl]phenyl}triaza-1,2-dien-2-ium
CAS No.:41657-69-6
Molecular Formula:C₁₆H₁₃N₃O₂
Molecular Weight:279.298
Hs Code.:
DSSTox Substance ID:DTXSID10700928

Synonyms:DTXSID10700928;1-{4-[3-(4-Methoxyphenyl)acryloyl]phenyl}triaza-1,2-dien-2-ium

Suppliers and Price of 1-{4-[3-(4-Methoxyphenyl)acryloyl]phenyl}triaza-1,2-dien-2-ium

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-{4-[3-(4-Methoxyphenyl)acryloyl]phenyl}triaza-1,2-dien-2-ium

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:280.108601698
Heavy Atom Count:21
Complexity:413

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=CC(=O)C2=CC=C(C=C2)N=[N+]=N

Technology Process of 1-{4-[3-(4-Methoxyphenyl)acryloyl]phenyl}triaza-1,2-dien-2-ium

There total 6 articles about 1-{4-[3-(4-Methoxyphenyl)acryloyl]phenyl}triaza-1,2-dien-2-ium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 123-11-5
4-methoxy-benzaldehyde

: 20062-24-2
4-azidoacetophenone

: 41657-69-6
(E)-1-(4-Azido-phenyl)-3-(4-methoxy-phenyl)-propenone

Guidance literature:: With sodium hydroxide; In methanol; at 25 ℃;
DOI:10.1016/j.bmc.2006.06.022

Reference yield: 70.0%

: 123-11-5
4-methoxy-benzaldehyde

: 20062-24-2
4-azidoacetophenone

: 41657-69-6
(E)-1-(4-Azido-phenyl)-3-(4-methoxy-phenyl)-propenone

Guidance literature:: With sodium hydroxide; for 2h;

Reference yield:

: 99-92-3
p-aminobenzophenone

: 41657-69-6
(E)-1-(4-Azido-phenyl)-3-(4-methoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaNO₂, 50percent HCl, 2) NaN₃ / 1) water, 0 deg C, 2) water

2: 70 percent / 33 percent NaOH / 2 h

With hydrogenchloride; sodium hydroxide; sodium azide; sodium nitrite;