[(2-Ethylcyclohex-1-en-1-yl)oxy](trimethyl)silane

Base Information

• Chemical Name: [(2-Ethylcyclohex-1-en-1-yl)oxy](trimethyl)silane
• CAS No.: 89683-95-4
• Molecular Formula: C11H22OSi
• Molecular Weight: 198.381
• DSSTox Substance ID: DTXSID10529095
• Nikkaji Number: J2.114.538F
• Wikidata: Q82399256
• Mol file: 89683-95-4.mol

Synonyms:89683-95-4;[(2-Ethylcyclohex-1-en-1-yl)oxy](trimethyl)silane;DTXSID10529095

Chemical Property of [(2-Ethylcyclohex-1-en-1-yl)oxy](trimethyl)silane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 198.143991855
• Heavy Atom Count: 13
• Complexity: 201

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1=C(CCCC1)O[Si](C)(C)C

Technology Process of [(2-Ethylcyclohex-1-en-1-yl)oxy](trimethyl)silane

There total 5 articles about [(2-Ethylcyclohex-1-en-1-yl)oxy](trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C12H23BO (89683-94-3) + 1-(Trimethylsilyl)imidazole (18156-74-6) → (2-ethylcyclohex-1-enyloxy)trimethylsilane (89683-95-4)

Guidance literature:

In tetrahydrofuran; -10 deg C to rt., overnight;

DOI:10.1016/S0040-4039(00)94175-3

Reference yield: 41.0%

chloro-trimethyl-silane (75-77-4) + 2-ethylcyclohexanone (4423-94-3) → (2-ethylcyclohex-1-enyloxy)trimethylsilane (89683-95-4)

Guidance literature:

chloro-trimethyl-silane; 2-ethylcyclohexanone; With triethylamine; sodium iodide; In acetonitrile; Inert atmosphere;

With oxygen; palladium diacetate; In dimethyl sulfoxide; for 48h; Darkness;

DOI:10.1002/chem.201003383

Reference yield:

(6-ethyl-cyclohex-1-enyloxy)-trimethyl-silane → (2-ethylcyclohex-1-enyloxy)trimethylsilane (89683-95-4)

Guidance literature:

With oxygen; palladium diacetate; In dimethyl sulfoxide; for 48h;

DOI:10.1021/ja044812x

upstream raw materials:

C₁₂H₂₃BO

1-(Trimethylsilyl)imidazole

chloro-trimethyl-silane

2-ethylcyclohexanone

Downstream raw materials:

(S)-2-allyl-2-ethylcyclohexanone

allyl 2-ethylcyclohex-1-enyl carbonate