3,3-Dimethyltricyclo[2.2.1.02,6]heptane

Base Information

• Chemical Name: 3,3-Dimethyltricyclo[2.2.1.02,6]heptane
• CAS No.: 473-02-9
• Molecular Formula: C9H14
• Molecular Weight: 122.21
• Mol file: 473-02-9.mol

Synonyms:Apocyclen;Tricyclo[2.2.1.02,6]heptane, 3,3-dimethyl-;(1R,2S,4R,6S)-3,3-Dimethyl-tricyclo[2.2.1.02,6]heptane;

Chemical Property of 3,3-Dimethyltricyclo[2.2.1.02,6]heptane

Chemical Property:

• Melting Point: 42.5°C
• Refractive Index: 1.4514
• Boiling Point: 162.66°C (rough estimate)
• PSA: 0.00000
• Density: 0.8710
• LogP: 2.29840

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3-Dimethyltricyclo[2.2.1.02,6]heptane

There total 7 articles about 3,3-Dimethyltricyclo[2.2.1.02,6]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

1-trymethylsilyl-7,7-dimethylbicyclo<2.2.1>heptan-2-ol (116417-15-3) → Hexamethyldisiloxane (107-46-0) + 3,3-dimethyl-2,6-cyclo-norbornane (473-02-9)

Guidance literature:

at 760 ℃; FVP (flash vacuum pyrolysis);

DOI:10.1016/S0040-4039(00)96877-1

Reference yield:

(1R)-7,7-Dimethylbicyclo<2.2.1>heptan-2-on-p-tolylsulfonylhydrazon (91573-14-7) → camphenilanol (5957-68-6) + 5,5-dimethyl-norbornan-2-ol (258264-50-5) + α-Isofenchocamphorol (91605-15-1) + 3,3-dimethyl-2,6-cyclo-norbornane (473-02-9) + 7,7-Dimethyl-exo-norbornanol (51153-09-4) + 2-(3-cyclohexenyl)-2-propanol (90645-55-9)

Guidance literature:

With sodium hydroxide; for 1.5h; Product distribution; Mechanism; Irradiation; further reagent: NaOCH₂Ph;

Reference yield:

(1R,2S,4S)-1-Dimethylsilanyl-7,7-dimethyl-bicyclo[2.2.1]heptan-2-ol (116417-16-4) → 1,1,3,3-Tetramethyldisiloxane (3277-26-7) + 3,3-dimethyl-2,6-cyclo-norbornane (473-02-9)

Guidance literature:

at 740 ℃; under 0.0005 Torr; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)96877-1

upstream raw materials:

camphenilanol

(1R,2S,4S)-1-Dimethylsilanyl-7,7-dimethyl-bicyclo[2.2.1]heptan-2-ol

1-trymethylsilyl-7,7-dimethylbicyclo<2.2.1>heptan-2-ol

(1R)-7,7-Dimethylbicyclo<2.2.1>heptan-2-on-p-tolylsulfonylhydrazon

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