Benzeneethanesulfinyl chloride

Base Information

• Chemical Name: Benzeneethanesulfinyl chloride
• CAS No.: 89986-79-8
• Molecular Formula: C₈H₉ClOS
• Molecular Weight: 188.678

Synonyms:

Chemical Property of Benzeneethanesulfinyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Benzeneethanesulfinyl chloride

There total 2 articles about Benzeneethanesulfinyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenethyl disulfide (27846-22-6) → 2-phenetyl sulfinyl chloride (89986-79-8)

Guidance literature:

With sulfuryl dichloride; acetic acid; at -20 - 35 ℃; for 6.5h;

DOI:10.1039/d1ob01714d

Reference yield:

S-2-phenylethyl thioacetate (35065-97-5) → 2-phenylethylsulfonyl chloride (4025-71-2) + 2-phenetyl sulfinyl chloride (89986-79-8)

Guidance literature:

With chlorine; In acetic anhydride; for 0.5h; Yield given. Yields of byproduct given;

Reference yield: 48.0%

2-phenetyl sulfinyl chloride (89986-79-8) + N-butylamine (109-73-9,85404-21-3) → n-butyl-2-phenylethane-1-sulfinamide

Guidance literature:

In dichloromethane; at -78 - 20 ℃; for 3h;

DOI:10.1039/d1ob01714d

upstream raw materials:

S-2-phenylethyl thioacetate

diphenethyl disulfide

Downstream raw materials:

2-phenylethylsulfonyl chloride

S-phenethyl 2-phenylethane-1-sulfonothioate

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