1-[(2-CHLOROETHYL)THIO]-4-METHYLBENZENE

Base Information

• Chemical Name: 1-[(2-CHLOROETHYL)THIO]-4-METHYLBENZENE
• CAS No.: 20761-71-1
• Molecular Formula: C9H11ClS
• Molecular Weight: 186.705
• Hs Code.: 2930909090
• Mol file: 20761-71-1.mol

Synonyms:(2-chloro-ethyl)-p-tolyl sulfide;(2-Chlor-aethyl)-p-tolyl-sulfid;4-(2-Chlor-aethylmercapto)-toluol;1-[(2-chloroethyl)thio]-4-methylbenzene;Sulfide,2-chloroethyl-p-tolyl;2-p-Tolylmercapto-aethylchlorid;2-Chlor-1-p-tolylmercapto-aethan;

Chemical Property of 1-[(2-CHLOROETHYL)THIO]-4-METHYLBENZENE

Chemical Property:

• Vapor Pressure: 0.0191mmHg at 25°C
• Boiling Point: 261.1°C at 760 mmHg
• Flash Point: 109.9°C
• PSA: 25.30000
• Density: 1.13g/cm³
• LogP: 3.32590

Purity/Quality:

99% ^*data from raw suppliers

1-[(2-chloroethyl)sulfanyl]-4-methylbenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[(2-CHLOROETHYL)THIO]-4-METHYLBENZENE

There total 9 articles about 1-[(2-CHLOROETHYL)THIO]-4-METHYLBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

para-thiocresol (106-45-6) + 2-chloro-ethanol (107-07-3) → (2-chloro-ethyl)-p-tolyl sulfide (20761-71-1)

Guidance literature:

para-thiocresol; With sodium ethanolate; In ethanol; at 20 ℃; for 0.5h;

2-chloro-ethanol; In ethanol; for 3.5h; Heating;

With hydrogenchloride; In ethanol; water; 15 h, r.t., 4.5 h, reflux;

DOI:10.1016/S0022-328X(00)00289-8

Reference yield:

2-(p-tolylthio)-ethanol (13290-16-9) → (2-chloro-ethyl)-p-tolyl sulfide (20761-71-1)

Guidance literature:

With pyridine; thionyl chloride;

Reference yield:

2-chloroethyl tosylate (80-41-1) + para-thiocresol (106-45-6) → (2-chloro-ethyl)-p-tolyl sulfide (20761-71-1)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

tetrachloromethane

p-methylbenzenesulfenyl chloride

ethene

2-(p-tolylthio)-ethanol

Downstream raw materials:

2-chloroethyl-p-toluenesulfonate

1-methyl-4-[(2-phenylethyl)sulfanyl]benzene

p-tolyl vinyl sulfide

1-iodo-2-(4-methylbenzenethio)ethane

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