4,7,10,13-Tetraoxahexadeca-1,15-diene

Base Information

• Chemical Name: 4,7,10,13-Tetraoxahexadeca-1,15-diene
• CAS No.: 90736-68-8
• Molecular Formula: C12H22O4
• Molecular Weight: 230.304
• DSSTox Substance ID: DTXSID60446884
• Nikkaji Number: J705.541B
• Wikidata: Q82265624

Synonyms:Propenyl-PEG3-Propenyl;90736-68-8;4,7,10,13-Tetraoxahexadeca-1,15-diene;3-[2-[2-(2-prop-2-enoxyethoxy)ethoxy]ethoxy]prop-1-ene;triethylene glycol diallyl ether;SCHEMBL177611;DTXSID60446884;1,2-Bis[2-(allyloxy)ethoxy]ethane;AKOS040758445;HY-134676;CS-0147947

Chemical Property of 4,7,10,13-Tetraoxahexadeca-1,15-diene

Chemical Property:

• XLogP3: 0.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 13
• Exact Mass: 230.15180918
• Heavy Atom Count: 16
• Complexity: 141

Purity/Quality:

99.3% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCOCCOCCOCCOCC=C

Technology Process of 4,7,10,13-Tetraoxahexadeca-1,15-diene

There total 2 articles about 4,7,10,13-Tetraoxahexadeca-1,15-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

allyl bromide (106-95-6) + 2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → 4,7,10,13-tetraoxahexadeca-1,15-diene (90736-68-8,59788-01-1)

Guidance literature:

2,2'-[1,2-ethanediylbis(oxy)]bisethanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere;

allyl bromide; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere;

DOI:10.1055/s-0037-1612249

Reference yield:

ethylene glycol monoallyl ether (111-45-5,27274-31-3) + 1,2-bis-tosyloxyethane (6315-52-2) → 4,7,10,13-tetraoxahexadeca-1,15-diene (90736-68-8,59788-01-1)

Guidance literature:

With potassium hydroxide; tetrabutylammomium bromide; In toluene; at 100 ℃; for 2h;

DOI:10.1055/s-2004-816007

Reference yield:

4,7,10,13-tetraoxahexadeca-1,15-diene (90736-68-8,59788-01-1) → ethoglucid (1954-28-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1080/10426507.2016.1255622

upstream raw materials:

ethylene glycol monoallyl ether

1,2-bis-tosyloxyethane

allyl bromide

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

Downstream raw materials:

ethoglucid

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