4-Phenylbut-2-YN-1-amine

Base Information

Chemical Name:4-Phenylbut-2-YN-1-amine
CAS No.:91375-44-9
Molecular Formula:C10H11N
Molecular Weight:145.20100
Hs Code.:
DSSTox Substance ID:DTXSID20580975
Wikidata:Q82471983

Synonyms:3-Benzylpropargylamine;4-PHENYLBUT-2-YN-1-AMINE;91375-44-9;SCHEMBL8826116;DTXSID20580975;IVGUVVWQZREBAF-UHFFFAOYSA-N;AKOS006337199

Suppliers and Price of 4-Phenylbut-2-YN-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 4-Phenylbut-2-YN-1-amine

Chemical Property:

Boiling Point:267.9±33.0 °C(Predicted)
PSA：26.02000
Density:1.020±0.06 g/cm3(Predicted)
LogP:1.89150
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:145.089149355
Heavy Atom Count:11
Complexity:154

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CC#CCN

Technology Process of 4-Phenylbut-2-YN-1-amine

There total 3 articles about 4-Phenylbut-2-YN-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 91375-43-8
1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-but-2-ynyl)-disilazane

: 91375-44-9
3-Benzylpropargylamine

Guidance literature:: With potassium fluoride; In methanol; for 3h;
DOI:10.1016/S0040-4020(01)88215-6

Reference yield:

: 100-39-0
benzyl bromide

: 91375-44-9
3-Benzylpropargylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) ether, THF, 30 min, r.t., 2.) THF, 40 deg C

2: 95 percent / KF / methanol / 3 h

With potassium fluoride; n-butyllithium; In methanol;
DOI:10.1016/S0040-4020(01)88215-6