1,1,1-Trimethyl-N-(4-phenylbut-2-yn-1-yl)-N-(trimethylsilyl)silanamine

Base Information

Chemical Name:1,1,1-Trimethyl-N-(4-phenylbut-2-yn-1-yl)-N-(trimethylsilyl)silanamine
CAS No.:91375-43-8
Molecular Formula:C16H27NSi2
Molecular Weight:289.568
Hs Code.:
DSSTox Substance ID:DTXSID50537194
Wikidata:Q82412113

Synonyms:91375-43-8;DTXSID50537194;1,1,1-Trimethyl-N-(4-phenylbut-2-yn-1-yl)-N-(trimethylsilyl)silanamine

Suppliers and Price of 1,1,1-Trimethyl-N-(4-phenylbut-2-yn-1-yl)-N-(trimethylsilyl)silanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,1,1-Trimethyl-N-(4-phenylbut-2-yn-1-yl)-N-(trimethylsilyl)silanamine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:289.16820293
Heavy Atom Count:19
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)N(CC#CCC1=CC=CC=C1)[Si](C)(C)C

Technology Process of 1,1,1-Trimethyl-N-(4-phenylbut-2-yn-1-yl)-N-(trimethylsilyl)silanamine

There total 2 articles about 1,1,1-Trimethyl-N-(4-phenylbut-2-yn-1-yl)-N-(trimethylsilyl)silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 91375-43-8
1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-but-2-ynyl)-disilazane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, 2.) H₂O, phosphate buffer / 1.) Et₂O, overnight

2: 1.) n-BuLi / 1.) ether, THF, 30 min, r.t., 2.) THF, 40 deg C

With n-butyllithium; phosphate buffer; water;
DOI:10.1016/S0040-4020(01)88215-6

Reference yield:

: 100-39-0
benzyl bromide

: 91375-25-6
1,1,1,3,3,3-hexamethyl-2-(prop-2-ynyl)disilazane

: 91375-43-8
1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-but-2-ynyl)-disilazane

: 144238-01-7
2-(4,5-Diphenyl-pent-2-ynyl)-1,1,1,3,3,3-hexamethyl-disilazane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, THF, 30 min, r.t., 2.) THF, 40 deg C;
DOI:10.1016/S0040-4020(01)88215-6